Gas Chromatography Analysis of Reaction Mixtures from Cycloaddition Reaction of α-Ethylacroleine and Ethyl Ester α-Ethylacrylic Acid

…, IP Polyuzhyn, GO Marshalok, YY Yatchyshyn

Index: Karpyak; Polyuzhyn; Marshalok; Yatchyshyn Polish Journal of Chemistry, 2008 , vol. 82, # 1-2 p. 397 - 401

Full Text: HTML

Citation Number: 2

Abstract

Résumé/Abstract The gas chromatography (GC) method was applied for the analysis of reaction mixture from synthesis of2-carboethoxy-2, 5-diethyl-3, 4-dihydro-2H-pyran. Relative errors of GC determinations not exceeded more than 7-8%. The reaction optimal conditions were proposed on the basis of such criteria as the conversion of α-ethylacrolein, yields and selectivities of main products by using the GC method.