Photochemistry of the Phthalimide System, 37. Thiazacycloalkanols by Photocyclization of S??Substituted N??(Thioalkyl) phthalimides

Y Sato, H Nakai, M Wada, T Mizoguchi…

Index: Sato, Yasuhiko; Nakai, Hideo; Wada, Masao; Mizoguchi, Tomishige; Hatanaka, Yasumaru; et al. Liebigs Annalen der Chemie, 1985 , # 6 p. 1099 - 1118

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Abstract

Abstract N-Substituted phthalimides (1, 2) possessing a terminal thioether function in their side chain were irradiated with a high-pressure mercury lamp to give a variety of thiazacycloalkanol derivatives (3, 7, 9–13, 16, 17) with favored γ-, δ-, ϵ-, and ζ-hydrogen abstractions (Table 1), in moderate to fairly good yields.

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