Direct Amide Synthesis from Alcohols and Amines by Phosphine??Free Ruthenium Catalyst Systems

SC Ghosh, S Muthaiah, Y Zhang, X Xu…

Index: Ghosh, Subhash Chandra; Muthaiah, Senthilkumar; Zhang, Yao; Xu, Xiangya; Hong, Soon Hyeok Advanced Synthesis and Catalysis, 2009 , vol. 351, # 16 p. 2643 - 2649

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Citation Number: 144

Abstract

Abstract Amides are synthesized directly from alcohols and amines in high yields using an in situ generated catalyst from easily available ruthenium complexes such as the (p-cymene) ruthenium dichloride dimer,[Ru (p-cymeme) Cl 2] 2, or the (benzene) ruthenium dichloride dimer,[Ru (benzene) Cl 2] 2, an N-heterocyclic carbene (NHC) ligand, and a nitrogen containing L-type ligand such as acetonitrile. The phosphine-free catalyst systems ...

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