3,5-Dimethylphenylboronic acid

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Names

[ Name ]:
3,5-Dimethylphenylboronic acid

[Synonym ]:
(3,5-Dimethylphenyl)boronic acid
3,5-Dimethylphenylboronic acid
3,5-dimethylphenyl boronic acid
m-Xylene-2-boronic Acid
2,6-Dimethylphenylboronic acid
(2,6-Dimethylphenyl)boronic acid
2,6-Dimethylbenzeneboronic Acid
Boronic acid, B-(2,6-dimethylphenyl)-
Boronic acid, B-(3,5-dimethylphenyl)-
MFCD01009693

Chemical & Physical Properties

[ Density]:
1.1±0.1 g/cm3

[ Boiling Point ]:
299.9±50.0 °C at 760 mmHg

[ Melting Point ]:
105 °C (dec.)(lit.)

[ Molecular Formula ]:
C₈H₁₁BO₂

[ Molecular Weight ]:
149.98

[ Flash Point ]:
135.2±30.1 °C

[ Exact Mass ]:
150.085205

[ PSA ]:
40.46000

[ LogP ]:
2.51

[ Vapour Pressure ]:
0.0±0.7 mmHg at 25°C

[ Index of Refraction ]:
1.523

[ Storage condition ]:
0-6°C

MSDS

Click to get detail MSDS

Safety Information

[ Personal Protective Equipment ]:
Eyeshields;Gloves;type N95 (US);type P1 (EN143) respirator filter

[ Hazard Codes ]:
Xn:Harmful;

[ Risk Phrases ]:
R22;R36/37/38

[ Safety Phrases ]:
S37/39-S26

[ RIDADR ]:
NONH for all modes of transport

[ WGK Germany ]:
3

[ HS Code ]:
2931900090

Synthetic Route

Click to get detail synthetic route

Precursor & DownStream

Precursor

Trimethyl borate
2,6-Dimethylbromobenzene
2,6-dimethylphenylmagnesium bromide
dimethoxy(2,6-dimethylphenyl)borone
3-Chloro-o-xylene

DownStream

m-xylene, 2-iodo-
2-Fluoro-1,3-dimethylbenzene
Fluoromesitylene
2-ethenyl-1,3-dimethylbenzene
ethyl 2-(2,6-dimethylphenyl)acetate
m-Xylene
1,3-dimethyl-2-(2-methylphenyl)benzene
2,6-xylidine
2,6-Xylenol
nitro m-xylene

Customs

[ HS Code ]: 2931900090

[ Summary ]:
2931900090. other organo-inorganic compounds. VAT:17.0%. Tax rebate rate:13.0%. Supervision conditions:AB(certificate of inspection for goods inward,certificate of inspection for goods outward). MFN tariff:6.5%. General tariff:30.0%

Articles

Highly efficient aerobic oxidative hydroxylation of arylboronic acids: photoredox catalysis using visible light.

Angew. Chem. Int. Ed. Engl. 3rd ed., 51 , 784-788, (2012)

Room-temperature synthesis of tetra-ortho-substituted biaryls by NHC-catalyzed Suzuki-Miyaura couplings.

Chemistry 46th ed., 17 , 12886-12890, (2011)

ipso-Nitration of arylboronic acids with bismuth nitrate and perdisulfate.

Org. Lett. 7th ed., 14 , 1736-1739, (2012)

An efficient and one pot synthetic method of ipso-nitration of arylboronic acids has been developed. The high efficiency, general applicability, and broader substrate scope including heterocycles and ...

3,5-Dimethylphenylboronic acid
3,5-Dimethylphenylboronic acid
4-Cyano-3,5-dimethylphenylboronic acid
4-Bromo-3,5-dimethylphenylboronic acid
2-Ethyl-3,5-Dimethylphenylboronic acid
4-Ethyl-3,5-Dimethylphenylboronic Acid
3-chloro-2-(4,5-dihydro-1H-imidazol-2-yl)-5-(trifluoromethyl)pyridine
1-(3-(3-Chloro-5-(trifluoromethyl)pyridin-2-yl)phenyl)ethanone
3-(3-Chloro-5-(trifluoromethyl)pyridin-2-yl)benzonitrile
3-Amino-5-[3-chloro-5-(trifluoromethyl)pyridin-2-yl]thieno[2,3-b]pyridine-2-carboxylic acid
Methyl 3,6'-dichloro-5-(trifluoromethyl)-[2,3'-bipyridine]-5'-carboxylate
Methyl 3-chloro-6'-methoxy-5-(trifluoromethyl)-[2,3'-bipyridine]-5'-carboxylate
3-Chloro-6'-methoxy-5-(trifluoromethyl)-[2,3'-bipyridine]-5'-carboxylic acid
2-(3-chloro-5-(trifluoromethyl)pyridin-2-yl)-2,2-difluoro-N-hydroxyacetamide
4-(3-chloro-5-(trifluoromethyl)pyridin-2-yl)-1-phenyl-1H-pyrazol-5-amine
methyl 2-(5-(3-chloro-5-(trifluoromethyl)pyridin-2-yl)-1H-1,2,4-triazol-1-yl)acetate

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