2-Methylamino-5-chlorobenzophenone

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Names

[ CAS No. ]:
1022-13-5

[ Name ]:
2-Methylamino-5-chlorobenzophenone

[Synonym ]:
Ro 5-4365
2-METHYLAMINO-5-CHLORO BENZOPHENONE
Methyl-aMino ketone
2-Methylamino-5-chlorobenzophenone
Benzophenone,2-acetamido-5-chloro
EINECS 213-822-1
Methanone, [5-chloro-2-(methylamino)phenyl]phenyl-
Diazepam,acid hydrolyzed
Diazepam benzophenone
[5-Chloro-2-(methylamino)phenyl](phenyl)methanone
(5-Chloro-2-(methylamino)phenyl)(phenyl)methanone
5-chloro-2-methylaminobenzophenone
TeMazepaM IMpurity A
MFCD00008284
5-Chloro-2-(Methylamino)Benzophenone
Benzophenone, 2-methylamino-5-chloro-

Chemical & Physical Properties

[ Density]:
1.2±0.1 g/cm3

[ Boiling Point ]:
421.9±35.0 °C at 760 mmHg

[ Melting Point ]:
93-95 °C(lit.)

[ Molecular Formula ]:
C14H12ClNO

[ Molecular Weight ]:
245.71

[ Flash Point ]:
209.0±25.9 °C

[ Exact Mass ]:
245.060745

[ PSA ]:
29.10000

[ LogP ]:
4.66

[ Vapour Pressure ]:
0.0±1.0 mmHg at 25°C

[ Index of Refraction ]:
1.627

[ Stability ]:
Stable. Incompatible with strong oxidizing agents.

MSDS

Click to get detail MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
DJ0414000
CHEMICAL NAME :
Benzophenone, 5-chloro-2-(methylamino)-
CAS REGISTRY NUMBER :
1022-13-5
LAST UPDATED :
199701
DATA ITEMS CITED :
2
MOLECULAR FORMULA :
C14-H12-Cl-N-O
MOLECULAR WEIGHT :
245.72

Safety Information

[ Symbol ]:

GHS07

[ Signal Word ]:
Warning

[ Hazard Statements ]:
H315-H319-H335

[ Precautionary Statements ]:
P305 + P351 + P338

[ Personal Protective Equipment ]:
dust mask type N95 (US);Eyeshields;Gloves

[ Hazard Codes ]:
Xi:Irritant;

[ Risk Phrases ]:
R36/37/38

[ Safety Phrases ]:
S26-S37/39

[ RIDADR ]:
NONH for all modes of transport

[ WGK Germany ]:
3

[ RTECS ]:
DJ0414000

[ HS Code ]:
2922399090

Synthetic Route

Click to get detail synthetic route

Precursor & DownStream

Precursor

  • 2-Amino-5-chlorobenzophenone
  • Dimethyl sulfate
  • N-methyl-3-phenyl-5-chloroanthranil methosulfate
  • N-(2-benzoyl-4-chlorophenyl)-N-methylacetamide
  • carbon monoxide
  • methyl iodide
  • N-(N-phthaloyl-DL-alanyl)-N'-methyl-2'-benzoyl-4'-chlorosarcosinanilide
  • Ethanol
  • 2-acetamido-N-(2-benzoyl-4-chlorophenyl)-N-methylacetamide
  • 2-(methylamino-acetamido)-5-chloro-benzophenone

DownStream

  • diazepam
  • 2-(N-methyl)amino-3,5-dichlorobenzophenone
  • (2-amino-3,5-dichlorophenyl)-phenylmethanone
  • (5-chloro-2-(dimethylamino)phenyl)(phenyl)methanone
  • 2-Amino-5-chlorobenzophenone
  • 6-chloro-1-methyl-4-phenyl-1H-benzo[1,2,6]thiadiazine 2,2-dioxide
  • 6-chloro-1-methyl-4-phenylquinazolin-2-one
  • 7-Chloro-1-methyl-3,4-dihydro-1H-benzo[e][1,4]diazepine-2,5-dione
  • 2-(N-Methylchloroacetyzamine)-5-chlorobenzophenone

Customs

[ HS Code ]: 2922399090

[ Summary ]:
2922399090 other amino-aldehydes, amino-ketones and amino-quinones, other than those containing more than one kind of oxygen function; salts thereof VAT:17.0% Tax rebate rate:9.0% Supervision conditions:none MFN tariff:6.5% General tariff:30.0%

Articles

Determination of hydrazine in pharmaceuticals IV: Hydrazine and benzylhydrazine in isocarboxazid.

J. Pharm. Sci. 74(1) , 105-7, (1985)

A GC procedure for the simultaneous determination of hydrazine and benzylhydrazine in isocarboxazid raw material and tablet formulations has been developed. The method is based on the reaction of benz...

[The preservability of sibazon breakdown products in the cadavers of experimental animals].

Sud. Med. Ekspert. 41(3) , 24-6, (1998)

Cibasone degradation products were measured in corpses of 15 cats poisoned with cibasone in a dose of 750 mg/kg. Cibasone was assessed by semiquantitative method on Silufol UV-254 plates from the cont...

Simplified method for simultaneous determination of diazepam and its metabolites in urine by thin-layer chromatography and direct densitometry.

J. Chromatogr. A. 615(2) , 365-8, (1993)

A direct densitometric method for determination of diazepam and its metabolites in urine was developed. The proposed procedure involves acid hydrolysis of urine specimens, thereby converting diazepam ...


More Articles

Related Compounds

  • 2-methylamino-5-chlorobenzophenone imine
  • N,5-Dimethylpyridin-2-amine
  • 2-(methylamino)-5-sulphobenzoic acid
  • 2-methylamino-5,2'-dichlorobenzhydrol
  • 2-(methylamino)-5-[[3-(trifluoromethyl)phenyl]methyl]-1,3-thiazol-4-one
  • [2-(methylamino)-5-morpholin-4-yl-1,3-oxazol-4-yl]-triphenylphosphanium,perchlorate