Methyl cyanoacetate

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Names

[ CAS No. ]:
105-34-0

[ Name ]:
Methyl cyanoacetate

[Synonym ]:
EINECS 203-288-8
Methylcyanoacetate
methyl 2-cyanoacetate
Acetic acid, 2-cyano-, methyl ester
Methyl cyanoacetate
Cyanoacetic acid methyl ester
MFCD00001939

Chemical & Physical Properties

[ Density]:
1.1±0.1 g/cm3

[ Boiling Point ]:
208.0±8.0 °C at 760 mmHg

[ Melting Point ]:
-13 °C

[ Molecular Formula ]:
C4H5NO2

[ Molecular Weight ]:
99.088

[ Flash Point ]:
86.5±5.2 °C

[ Exact Mass ]:
99.032028

[ PSA ]:
50.09000

[ LogP ]:
-0.47

[ Vapour density ]:
3.41 (vs air)

[ Vapour Pressure ]:
0.2±0.4 mmHg at 25°C

[ Index of Refraction ]:
1.402

[ Water Solubility ]:
54 g/L (20 ºC)

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
AG4375000
CHEMICAL NAME :
Acetic acid, cyano-, methyl ester
CAS REGISTRY NUMBER :
105-34-0
BEILSTEIN REFERENCE NO. :
0773945
LAST UPDATED :
199701
DATA ITEMS CITED :
4
MOLECULAR FORMULA :
C4-H5-N-O2
MOLECULAR WEIGHT :
99.10
WISWESSER LINE NOTATION :
NC1VO1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
200 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
NTIS** National Technical Information Service. (Springfield, VA 22161) Formerly U.S. Clearinghouse for Scientific & Technical Information. Volume(issue)/page/year: AD277-689
TYPE OF TEST :
LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - guinea pig
DOSE/DURATION :
400 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
85JCAE "Prehled Prumyslove Toxikologie; Organicke Latky," Marhold, J., Prague, Czechoslovakia, Avicenum, 1986 Volume(issue)/page/year: -,920,1986 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - X4945 No. of Facilities: 17 (estimated) No. of Industries: 1 No. of Occupations: 1 No. of Employees: 1327 (estimated) No. of Female Employees: 255 (estimated)

Safety Information

[ Symbol ]:

GHS07

[ Signal Word ]:
Warning

[ Hazard Statements ]:
H319

[ Precautionary Statements ]:
P305 + P351 + P338

[ Personal Protective Equipment ]:
Eyeshields;Gloves

[ Hazard Codes ]:
Xi: Irritant;

[ Safety Phrases ]:
S24/25

[ RIDADR ]:
3276

[ WGK Germany ]:
1

[ RTECS ]:
AG4375000

[ Packaging Group ]:
III

[ Hazard Class ]:
6.1(b)

[ HS Code ]:
2926909090

Synthetic Route

Precursor & DownStream

Precursor

  • 3-Methoxypropionitrile
  • Methanol
  • Cyanoacetic acid
  • methyl 2-formamidoacetate
  • Ethyl cyanoacetate
  • Chloromethane
  • 2-Cyanoacetamide
  • dimethyl 2,3-dicyanobut-2-enedioate
  • Malononitrile
  • Sodium cyanide

DownStream

  • N,N''-DIBENZYL-MALONAMIDE
  • methyl 2-amino-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate,hydrochloride
  • 4-Nitrophenol
  • methyl 4-acetamido-2-cyano-3-oxobutanoate
  • 2-cyano-N-[3-[(2-cyanoacetyl)amino]propyl]acetamide
  • methyl 2-cyanooct-2-enoate
  • (5,6-DIHYDRO-4H-[1,3]THIAZIN-2-YL)-(2,5-DIMETHOXY-PHENYL)-AMINE
  • AC-BETA-ALA-OME
  • 2-AMINO-4-NAPHTHALEN-2-YL-THIOPHENE-3-CARBOXYLIC ACID METHYL ESTER
  • oxazolidinone

Customs

[ HS Code ]: 2926909090

[ Summary ]:
HS:2926909090 other nitrile-function compounds VAT:17.0% Tax rebate rate:9.0% Supervision conditions:none MFN tariff:6.5% General tariff:30.0%

Articles

The EpiOcular Eye Irritation Test (EIT) for hazard identification and labelling of eye irritating chemicals: protocol optimisation for solid materials and the results after extended shipment.

Altern. Lab. Anim. 43 , 101-27, (2015)

The 7th Amendment to the EU Cosmetics Directive and the EU REACH Regulation have reinforced the need for in vitro ocular test methods. Validated in vitro ocular toxicity tests that can predict the hum...

Calcite and fluorite as catalyst for the Knövenagel condensation of malononitrile and methyl cyanoacetate under solvent-free conditions. Wada S and Suzuki H.

Tetrahedron Lett. 44(2) , 399-401, (2003)

Conformational isomerism in methyl cyanoacetate: A combined matrix-isolation infrared spectroscopy and molecular orbital study. Reva ID, et al

Phys. Chem. Chem. Phys. 3(19) , 4235-4241, (2011)


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Related Compounds

  • 5-methylhexan-2-yl 2-cyanoacetate
  • methyl 2-(4-nitrophenyl)cyanoacetate
  • methyl 2-acetamido-2-cyanoacetate
  • methyl [(2-acetoxyphenyl)hydroxymethylidene]cyanoacetate
  • methyl 2-amino-2-cyanoacetate
  • methyl 2,2-dichloro-2-cyanoacetate
  • 4-((Cyclohexylamino)methyl)benzoic acid hydrochloride
  • 1-[(2,4-Dichlorophenyl)methyl]-N-(1,1-dimethylethyl)-2-methyl-1H-indole-3-methanamine
  • 4-[4-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)cyclopent-2-ene-1-amido]-3-methyloxolane-3-carboxylic acid
  • 5-Fluoro-6-propan-2-yl-2-[4-([1,2,4]triazolo[4,3-b]pyridazin-6-yl)piperazin-1-yl]-1,3-diazinan-4-one
  • 2-Methoxy-6-(pyrazol-1-yl)-benzonitrile
  • 1H-3-Benzazepin-7-ol, 8-chloro-2,3,4,5-tetrahydro-5-(3-iodophenyl)-3-methyl-, (S)-
  • (4-Methyl-tetrahydro-furan-2-yl)-methanol
  • N-(1-cyanocyclopentyl)-2-[4-(4-fluorobenzenesulfonyl)-1,4-diazepan-1-yl]acetamide
  • 4,5,6,7-Tetrahydrobenzo[d]isoxazole-3-carbaldehyde
  • tert-Butyl-DL-alanine