3,3'-Dimethoxybiphenyl-4,4'-diamine

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Names

[ CAS No. ]:
119-90-4

[ Name ]:
3,3'-Dimethoxybiphenyl-4,4'-diamine

[Synonym ]:
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethoxy-
3,3'-Dimethoxy-4,4'-diaminodiphenyl
3,3'-Dimethoxybenzidine
3,3‘-Dimethoxybenzidine
3,3'-Dimethoxy-4,4'-biphenyldiamine
4,4'-Diamino-3,3'-dimethoxybiphenyl
EINECS 204-355-4
3,3'-Dimethoxy-[1,1'-biphenyl]-4,4'-diamine
3,3'-Dimethoxybiphenyl-4,4'-diamine
Fast Blue B
3,3-Dimethoxybenzidine
MFCD00008372
o-dianisidine
4-(4-amino-3-methoxyphenyl)-2-methoxyaniline
3,3′-Dimethoxybenzidine

Chemical & Physical Properties

[ Density]:
1.2±0.1 g/cm3

[ Boiling Point ]:
391.3±37.0 °C at 760 mmHg

[ Melting Point ]:
137-138 °C(lit.)

[ Molecular Formula ]:
C14H16N2O2

[ Molecular Weight ]:
244.289

[ Flash Point ]:
206.1±0.0 °C

[ Exact Mass ]:
244.121185

[ PSA ]:
70.50000

[ LogP ]:
1.58

[ Vapour Pressure ]:
0.0±0.9 mmHg at 25°C

[ Index of Refraction ]:
1.619

[ Water Solubility ]:
H2O: slightly soluble

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
DD0875000
CHEMICAL NAME :
Benzidine, 3,3'-dimethoxy-
CAS REGISTRY NUMBER :
119-90-4
LAST UPDATED :
199710
DATA ITEMS CITED :
36
MOLECULAR FORMULA :
C14-H16-N2-O2
MOLECULAR WEIGHT :
244.32
WISWESSER LINE NOTATION :
1OR BZ ER DZ CO1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
1920 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Mammal - dog
DOSE/DURATION :
600 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
12 gm/kg/56W-I
TOXIC EFFECTS :
Tumorigenic - equivocal tumorigenic agent by RTECS criteria Sense Organs and Special Senses (Ear) - effect, not otherwise specified Skin and Appendages - tumors
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - hamster
DOSE/DURATION :
588 gm/kg/70W-C
TOXIC EFFECTS :
Tumorigenic - equivocal tumorigenic agent by RTECS criteria Kidney, Ureter, Bladder - tumors
TYPE OF TEST :
Mutation test systems - not otherwise specified
TYPE OF TEST :
Cytogenetic analysis

MUTATION DATA

TYPE OF TEST :
DNA adduct
TEST SYSTEM :
Mammal - dog Cells - not otherwise specified
REFERENCE :
CNREA8 Cancer Research. (Public Ledger Building, Suit 816, 6th & Chestnut Sts., Philadelphia, PA 19106) V.1- 1941- Volume(issue)/page/year: 44,1893,1984 *** REVIEWS *** IARC Cancer Review:Animal Sufficient Evidence IMEMDT IARC Monographs on the Evaluation of Carcinogenic Risk of Chemicals to Man. (WHO Publications Centre USA, 49 Sheridan Ave., Albany, NY 12210) V.1- 1972- Volume(issue)/page/year: 4,41,1974 IARC Cancer Review:Human Inadequate Evidence IMSUDL IARC Monographs, Supplement. (WHO Publications Centre USA, 49 Sheridan Ave., Albany, NY 12210) No.1- 1979- Volume(issue)/page/year: 7,198,1987 IARC Cancer Review:Group 2B IMSUDL IARC Monographs, Supplement. (WHO Publications Centre USA, 49 Sheridan Ave., Albany, NY 12210) No.1- 1979- Volume(issue)/page/year: 7,198,1987 TOXICOLOGY REVIEW AEHLAU Archives of Environmental Health. (Heldref Pub., 4000 Albemarle St., NW, Washington, DC 20016) V.1- 1960- Volume(issue)/page/year: 23,6,1971 TOXICOLOGY REVIEW ADCSAJ Advances in Chemistry Series. (American Chemical Soc., Distribution Office Dept. 223, POB 57136, West End Stn., Washington, DC 20037) No.1- 1950- Volume(issue)/page/year: 13,271,1970 *** OCCUPATIONAL EXPOSURE LIMITS *** OEL-FINLAND;Carcinogen JAN 1993 OEL-FRANCE;Carcinogen JAN 1993 OEL-GERMANY;Carcinogen JAN 1993 OEL-SWEDEN;Carcinogen JAN 1993 OEL-SWITZERLAND;Carcinogen JAN 1993 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH RECOMMENDED EXPOSURE LEVEL (REL) : NIOSH REL TO o-DIANISIDINE-BASED DYES-air:CA lowest feasible conc. REFERENCE : NIOSH* National Institute for Occupational Safety and Health, U.S. Dept. of Health, Education, and Welfare, Reports and Memoranda. Volume(issue)/page/year: DHHS #92-100,1992 NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOHS - National Occupational Hazard Survey (1974) NOHS Hazard Code - 80274 No. of Facilities: 49 (estimated) No. of Industries: 2 No. of Occupations: 3 No. of Employees: 122 (estimated) NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - 80274 No. of Facilities: 92 (estimated) No. of Industries: 4 No. of Occupations: 11 No. of Employees: 2481 (estimated) No. of Female Employees: 866 (estimated)

Safety Information

[ Symbol ]:

GHS07, GHS08

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H302-H350

[ Precautionary Statements ]:
P201-P308 + P313

[ Personal Protective Equipment ]:
Eyeshields;full-face particle respirator type N100 (US);Gloves;respirator cartridge type N100 (US);type P1 (EN143) respirator filter;type P3 (EN 143) respirator cartridges

[ Hazard Codes ]:
T:Toxic;

[ Risk Phrases ]:
R45;R22

[ Safety Phrases ]:
S53-S45

[ RIDADR ]:
2811

[ WGK Germany ]:
3

[ RTECS ]:
DD0875000

[ Packaging Group ]:
II

[ Hazard Class ]:
6.1(a)

[ HS Code ]:
2922299090

Synthetic Route

Precursor & DownStream

Precursor

  • 2,2'-Dimethoxyhydrazobenzene
  • nitroanisole
  • bis(2-methoxyphenyl)diazene
  • 2-Anisidine
  • 3,3',3'',3'''-tetramethoxy-4',4'''-azo-bis-biphenyl-4-ylamine
  • 2,2'-DIMETHOXYAZOXYBENZENE
  • Hydrochloric acid
  • molecular iodine
  • Sulfurous Acid

DownStream

  • [1,1'-Biphenyl]-4,4'-bis(diazonium),3,3'-dimethoxy-, chloride (1:2)
  • 1,1'-Biphenyl,4,4'-diisocyanato-3,3'-dimethoxy-
  • 1-Naphthalenesulfonicacid,3,3'-[(3,3'-dimethoxy[1,1'-biphenyl]-4,4'-diyl)bis(2,1-diazenediyl)]bis[4-hydroxy-,sodium salt (1:2)
  • 4,4'-Diamino-3,3'-biphenyldiol
  • 4,4'-diamino-3'-methoxy-biphenyl-3-ol
  • 1,1'-Biphenyl, 3,3'-dimethoxy-
  • Quinhydrone
  • 1-bromo-4-methoxy-2-(3-methoxyphenyl)benzene
  • 4-methoxy-2-(3-methoxyphenyl)benzoic acid
  • N,N'-Diacetyldianisidine

Customs

[ HS Code ]: 2922299090

[ Summary ]:
2922299090. other amino-naphthols and other amino-phenols, other than those containing more than one kind of oxygen function, their ethers and esters; salts thereof. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:30.0%

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Related Compounds

  • 3,3'-dimethoxybiphenyl-4,4'-diamine dihydrochloride
  • N,N'-Bis(2,4-dinitrophenyl)-3,3'-dimethoxybiphenyl-4,4'-diamine
  • 2,2'-DICHLORO-5,5'-DIMETHOXYBENZIDINE
  • diethyl 2-[[4-[4-[2-(1,3-diethoxy-1,3-dioxopropan-2-ylidene)hydrazinyl]-3-methoxyphenyl]-2-methoxyphenyl]hydrazinylidene]propanedioate
  • 4,4'-diiodo-3,3'-dimethoxybiphenyl
  • Tetrazolium blue
  • 4-((Cyclohexylamino)methyl)benzoic acid hydrochloride
  • 1-[(2,4-Dichlorophenyl)methyl]-N-(1,1-dimethylethyl)-2-methyl-1H-indole-3-methanamine
  • 2-Methoxy-6-(pyrazol-1-yl)-benzonitrile
  • 1H-3-Benzazepin-7-ol, 8-chloro-2,3,4,5-tetrahydro-5-(3-iodophenyl)-3-methyl-, (S)-
  • (4-Methyl-tetrahydro-furan-2-yl)-methanol
  • 1-(6-Amino-2-chloropyridin-3-yl)-2-bromoethanone;dihydrobromide
  • [5-(3-Chlorophenyl)-pyridin-3-ylmethyl]-methylamine
  • N-(1-cyanocyclopentyl)-2-[4-(4-fluorobenzenesulfonyl)-1,4-diazepan-1-yl]acetamide
  • Ethyl 4-chloro-6-methyl-1,7-naphthyridine-2-carboxylate
  • 4,5,6,7-Tetrahydrobenzo[d]isoxazole-3-carbaldehyde