2-chlorophenyl phosphorodichloridate

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Names

[ CAS No. ]:
15074-54-1

[ Name ]:
2-chlorophenyl phosphorodichloridate

[Synonym ]:
2-Chlorophenyl phosphorodichloridate
MFCD00009704
2-Chlorophenyl Phosphorodichloridate [Phosphorylating Agent]
EINECS 239-129-4
1-chloro-2-dichlorophosphoryloxybenzene

Chemical & Physical Properties

[ Density]:
1.491 g/mL at 25 °C(lit.)

[ Boiling Point ]:
135-137 °C12 mm Hg(lit.)

[ Molecular Formula ]:
C6H4Cl3O2P

[ Molecular Weight ]:
245.42800

[ Flash Point ]:
221 °F

[ Exact Mass ]:
243.90100

[ PSA ]:
36.11000

[ LogP ]:
4.30450

[ Vapour Pressure ]:
0.0113mmHg at 25°C

[ Index of Refraction ]:
n20/D 1.538(lit.)

[ Storage condition ]:
2-8°C

MSDS

Click to get detail MSDS

Safety Information

[ Symbol ]:

GHS05

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H314

[ Precautionary Statements ]:
P280-P305 + P351 + P338-P310

[ Personal Protective Equipment ]:
Faceshields;full-face respirator (US);Gloves;Goggles;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ Hazard Codes ]:
C: Corrosive;

[ Risk Phrases ]:
R34

[ Safety Phrases ]:
S26-S36/37/39-S45

[ RIDADR ]:
UN 3265 8/PG 2

[ WGK Germany ]:
3

[ Packaging Group ]:
II

[ Hazard Class ]:
8

[ HS Code ]:
2931900090

Synthetic Route

Click to get detail synthetic route

Precursor & DownStream

Precursor

  • 2-Chlorophenol
  • Sodium 2-chlorophenolate

DownStream

  • 2-Chlorophenol
  • 1,2-Dichlorobenzene
  • Phosphoric acid,2-chlorophenyl diphenyl ester
  • 1-[(2-chlorophenoxy)-(1,2,4-triazol-1-yl)phosphoryl]-1,2,4-triazole

Customs

[ HS Code ]: 2931900090

[ Summary ]:
2931900090. other organo-inorganic compounds. VAT:17.0%. Tax rebate rate:13.0%. Supervision conditions:AB(certificate of inspection for goods inward,certificate of inspection for goods outward). MFN tariff:6.5%. General tariff:30.0%

Articles

J. Chem. Soc. Perkin Trans. I , 2291, (1993)

Dealkylation of nucleoside arylmethyl 2-chlorophenyl phosphates: the 2, 4-dinitrobenzyl protecting group. Christadoulou C and Reese CB.

Tetrahedron Lett. 24(9) , 951-54, (1983)

A new approach to the synthesis of oligonucleotides and their phosphorothioate analogues in solution. Reese CB and Song Q.

Bioorg. Med. Chem. Lett. 7(21) , 2787-92, (1997)


More Articles

Related Compounds

  • (2-Chlorophenyl) phenyl sulfone
  • (2-chlorophenyl)-[5-fluoro-2-(hydroxymethyl)phenyl]methanone
  • 2-chlorophenyl (Z)-1-propenyl ether
  • (2-chlorophenyl)-(4-methoxy-3-methylphenyl)methanone
  • (2-chlorophenyl) ethenesulfonate
  • (2-chlorophenyl)methyl 2-(2-chlorophenyl)acetate
  • 2-((3-(4-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl)thio)-N-(2-(trifluoromethyl)phenyl)acetamide
  • 5-(2-Furanyl)-N-phenyl-1,3,4-thiadiazol-2-amine
  • 2-((3-(4-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl)thio)-N-(4-(trifluoromethyl)phenyl)acetamide
  • Ethyl 4-(2-((3-(4-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl)thio)acetamido)benzoate
  • Methyl 4-(2-((3-(4-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl)thio)acetamido)benzoate
  • N-(3-acetamidophenyl)-2-((3-(4-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl)thio)acetamide
  • N-cyclohexyl-2-((3-(4-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl)thio)acetamide
  • 3-(Methylamino)-6-(4-pyridinyl)-4-pyridazinecarboxamide
  • N-(2-chlorobenzyl)-2-((3-(4-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl)thio)acetamide
  • 1-Butyl-5-methyl-1H-pyrazol-4-amine
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