d8-tetrahydrofuran

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Names

[ Name ]:
d8-tetrahydrofuran

[Synonym ]:
(H)Tetrahydrofuran
perdeuteriotetrahydrofuran
Octadeuterotetrahydrofuran
d8-tetrahydrofuran
EINECS 216-898-4
Tetrahydrofuran-d8
Deuterated tetrahydrofuran
MFCD00044238
Furan-d, tetrahydro-d-

Chemical & Physical Properties

[ Density]:
0.9±0.1 g/cm3

[ Boiling Point ]:
68.3±8.0 °C at 760 mmHg

[ Melting Point ]:
-106ºC

[ Molecular Formula ]:
C₄D₈O

[ Molecular Weight ]:
80.155

[ Flash Point ]:
-17.2±0.0 °C

[ Exact Mass ]:
80.107727

[ PSA ]:
9.23000

[ LogP ]:
0.33

[ Vapour Pressure ]:
152.4±0.1 mmHg at 25°C

[ Index of Refraction ]:
1.417

[ Storage condition ]:
Refrigerator (+4°C)

[ Stability ]:
Stable. Incompatible with strong oxidizing agents, strong reducing agents, strong bases, oxygen. May generate peroxides in storage if in contact with air. Highly flammable. Store under nitrogen. Hazardous polymerisation may occur.

MSDS

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Safety Information

[ Symbol ]:

GHS02, GHS07, GHS08

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H225-H315-H319-H351

[ Precautionary Statements ]:
P210-P281-P305 + P351 + P338

[ Hazard Codes ]:
F:Highlyflammable;Xi:Irritant;

[ Risk Phrases ]:
R11;R19;R36/37

[ Safety Phrases ]:
S16-S29-S33

[ RIDADR ]:
UN 2056 3/PG 2

[ WGK Germany ]:
3

[ RTECS ]:
LU5950000

[ Packaging Group ]:
II

[ Hazard Class ]:
3.0

Synthetic Route

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Precursor & DownStream

Precursor

DownStream

ether
(3-ethylphenyl)-trimethyl-silane
(4-ethylphenyl)-trimethyl-silane
(butan-2-yl-3,3,4,4-d4)benzene
trimethyl((5-phenylhexyl-1,1,2,2,3,3,4,4-d8)oxy)silane
5-phenylhexan-1,1,2,2,3,3,4,4-d8-1-ol
Butylbenzene
4-Phenylbutan-1-ol
trimethyl(4-phenylbutoxy)silane

Articles

Syntheses, structures, and (1)H, (13)C{(1)H} and (119)Sn{(1)H} NMR chemical shifts of a family of trimethyltin alkoxide, amide, halide and cyclopentadienyl compounds.

Dalton Trans. 44 , 16156-63, (2015)

The synthesis and full characterization, including Nuclear Magnetic Resonance (NMR) data ((1)H, (13)C{(1)H} and (119)Sn{(1)H}), for a series of Me3SnX (X = O-2,6-(t)Bu2C6H3 (), (Me3Sn)N(2,6-(i)Pr2C6H3...

NMR lineshape theory of superimposed intermolecular spin exchange reactions and its action to the system acetic acid/methanol/tetrahydrofuran-d₈. Limbach HH.

J. Magn. Reson. 36(3) , 287-300, (1979)

Preparation and hydrogen-deuterium exchange of alkyl and hydride bis(trimethylsilyl) amido derivatives of the actinide elements. Simpson SJ, et al.

Inorg. Chem. 20(9) , 2991-2995, (1981)