9-Fluorenylmethyl carbazate

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Names

[ Name ]:
9-Fluorenylmethyl carbazate

[Synonym ]:
Fmoc-hydrazide
Fmoc-hydrazine
(9H-Fluoren-9-yl)methyl hydrazinecarboxylate
Fmoc-NHNH2
9-Fluorenylmethyl Carbazate
[(9H-Fluoren-9-ylmethoxy)carbonyl]hydrazine
Carbazic Acid 9-Fluorenylmethyl Ester
9H-Fluoren-9-ylmethyl hydrazinecarboxylate
Hydrazinecarboxylic acid, 9H-fluoren-9-ylmethyl ester
N-[(9H-fluoren-9-ylmethoxy)-carbonyl]-hydrazine
9-Fluorenylmethylcarbazate

Chemical & Physical Properties

[ Density]:
1.3±0.1 g/cm3

[ Boiling Point ]:
485.8±14.0 °C at 760 mmHg

[ Melting Point ]:
-170ºC (dec.)

[ Molecular Formula ]:
C₁₅H₁₄N₂O₂

[ Molecular Weight ]:
254.284

[ Flash Point ]:
247.6±20.1 °C

[ Exact Mass ]:
254.105530

[ PSA ]:
64.35000

[ LogP ]:
2.88

[ Vapour Pressure ]:
0.0±1.2 mmHg at 25°C

[ Index of Refraction ]:
1.632

[ Storage condition ]:
2-8°C

MSDS

Click to get detail MSDS

Safety Information

[ Symbol ]:

GHS07

[ Signal Word ]:
Warning

[ Hazard Statements ]:
H315-H319-H335

[ Precautionary Statements ]:
P261-P305 + P351 + P338

[ Personal Protective Equipment ]:
dust mask type N95 (US);Eyeshields;Gloves

[ Hazard Codes ]:
Xi: Irritant;

[ Risk Phrases ]:
R36/37/38

[ Safety Phrases ]:
26-36

[ RIDADR ]:
NONH for all modes of transport

[ WGK Germany ]:
3

[ HS Code ]:
2928000090

Synthetic Route

Click to get detail synthetic route

Precursor & DownStream

Precursor

9-Fluorenylmethyl chloroformate
9-Fluorenemethanol
Fmoc-Osu

DownStream

Customs

[ HS Code ]: 2928000090

[ Summary ]:
2928000090 other organic derivatives of hydrazine or of hydroxylamine VAT:17.0% Tax rebate rate:9.0% Supervision conditions:none MFN tariff:6.5% General tariff:20.0%

Articles

Synthesis and application of Fmoc-hydrazine for the quantitative determination of saccharides by reversed-phase high-performance liquid chromatography in the low and subpicomole range.

Anal. Biochem. 195 , 160, (1991)

A new derivatization reagent, Fmoc-hydrazine, has been synthesized from the reaction of Fmoc-chloroformate with hydrazine as a precolumn fluorometric labeling reagent for reducing sugars such as gluco...

Simple and sensitive multi-sugar-probe gut permeability test by high-performance liquid chromatography with fluorescence labelling.

J. Chromatogr. A. 730(1-2) , 99-105, (1996)

Enteral intake of a mixture of inert, non-metabolic monosaccharide and disaccharide probes, followed by measurement of their urinary probe ratio, is a well known method to investigate gut permeability...

A sensitive fluorescence reagent for the determination of aldehydes from alcoholic beverage using high-performance liquid chromatography with fluorescence detection and mass spectrometric identification.

Anal. Chim. Acta 636(1) , 95-104, (2009)

A pre-column derivatization method for the sensitive determination of aldehydes using the tagging reagent 2-[2-(7H-dibenzo[a,g] carbazol-7-yl)-ethoxy] ethyl carbonylhydrazine (DBCEEC) followed by high...

9-Fluorenylmethyl N-p-chlorphenyl carbamate
9-fluorenylmethyl 4,6-dimethoxy-1,3,5-triazinyl carbonate
9-fluorenylmethyl 3-nitro-1H-1,2,4-triazole-1-carboxylate
9-FLUORENYLMETHYL N-(2-AMINOETHYL)CARBAMATE HYDROBROMIDE
9-fluorenylmethyl 3,5-dichloro-2-hydroxy-4-methylphenylcarbamate
9-fluorenylmethyl N-(N-(2-dansyl)-2-aminoethyl)-carbamate
1-(2-Nitro-3-(trifluoromethylthio)phenyl)propan-1-one
1-(3,5-Bis(trifluoromethylthio)phenyl)propan-1-one
1-(2,3-Bis(methylthio)phenyl)-1-bromopropan-2-one
1-(3-(Bromomethyl)-2-mercaptophenyl)propan-1-one
1-(2-Amino-4-(difluoromethyl)phenyl)-3-bromopropan-2-one
1-(3-Amino-5-methoxyphenyl)-3-chloropropan-2-one
1-(3-Amino-5-(trifluoromethylthio)phenyl)-3-chloropropan-1-one
1-(3-(Difluoromethoxy)-2-(methylthio)phenyl)propan-1-one
1-(2-Amino-5-fluorophenyl)-3-bromopropan-2-one
1-(2-Amino-3-(trifluoromethylthio)phenyl)-3-bromopropan-2-one

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