(6aR,9R)-N,N-diethyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinoline-9-carboxamide

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Names

[ CAS No. ]:
35779-43-2

[ Name ]:
(6aR,9R)-N,N-diethyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinoline-9-carboxamide

[Synonym ]:
N-Demethyl-LSD
6-norlysergic
N-Demthyl-lsd
N-Demethyllysergic acid diethylamide
6-Norlysergic acid diethylamide
9,10-didehydro-ergoline-8-carboxylic acid diethylamide
nor-lysergic acid diethylamide
BIDD:GT0518

Chemical & Physical Properties

[ Density]:
1.23 g/cm3

[ Boiling Point ]:
550ºC at 760 mmHg

[ Molecular Formula ]:
C19H23N3O

[ Molecular Weight ]:
309.40500

[ Exact Mass ]:
309.18400

[ PSA ]:
48.13000

[ LogP ]:
2.89260

[ Index of Refraction ]:
1.657

Safety Information

[ Symbol ]:

GHS06

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H301-H311-H331

[ Precautionary Statements ]:
P261-P280-P301 + P310-P311

[ Personal Protective Equipment ]:
Eyeshields;Faceshields;Gloves;type P2 (EN 143) respirator cartridges

[ Hazard Codes ]:
T: Toxic;

[ Risk Phrases ]:
R23/24/25

[ Safety Phrases ]:
36/37/39-45

[ RIDADR ]:
UN 2811 6

[ HS Code ]:
2933990090

Synthetic Route

Click to get detail synthetic route

Precursor & DownStream

Precursor

  • lsd
  • 9,10-didehydro-N,N-diethyl-6-cyanoergoline-8β-carboxamide

DownStream

  • lsd
  • (6aR,9R)-N,N-diethyl-7-prop-2-enyl-6,6a,8,9-tetrahydro-4H-indolo[4,3-fg]quinoline-9-carboxamide

Customs

[ HS Code ]: 2933990090

[ Summary ]:
2933990090. heterocyclic compounds with nitrogen hetero-atom(s) only. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%

Articles

Quantification of LSD and N-demethyl-LSD in urine by gas chromatography/resonance electron capture ionization mass spectrometry.

Anal. Chem. 60(14) , 1420-5, (1988)

Determination of LSD and N-demethyl-LSD in urine by liquid chromatography coupled to electrospray ionization mass spectrometry.

J. Chromatogr. B. Biomed. Sci. Appl. 692(2) , 329-35, (1997)

A sensitive and highly specific method for the determination of LSD and N-demethyl-LSD in urine, using combined liquid chromatography and mass spectrometry (LC-MS) with electrospray ionization, has be...

Automated extraction of lysergic acid diethylamide (LSD) and N-demethyl-LSD from blood, serum, plasma, and urine samples using the Zymark RapidTrace with LC/MS/MS confirmation.

J. Forensic Sci. 43(3) , 622-5, (1998)

A forensic procedure for the quantitative confirmation of lysergic acid diethylamide (LSD) and the qualitative confirmation of its metabolite, N-demethyl-LSD, in blood, serum, plasma, and urine sample...


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