2,3-Dibromo-1-propanol

Suppliers

Names

[ CAS No. ]:
96-13-9

[ Name ]:
2,3-Dibromo-1-propanol

[Synonym ]:
2,3-dibromopropan-1-ol
MFCD00004699
EINECS 202-480-9

Chemical & Physical Properties

[ Density]:
2.12 g/mL at 25 °C(lit.)

[ Boiling Point ]:
95-97 °C10 mm Hg(lit.)

[ Melting Point ]:
8ºC

[ Molecular Formula ]:
C3H6Br2O

[ Molecular Weight ]:
217.88700

[ Flash Point ]:
>230 °F

[ Exact Mass ]:
215.87900

[ PSA ]:
20.23000

[ LogP ]:
1.13710

[ Index of Refraction ]:
n20/D 1.559(lit.)

[ Water Solubility ]:
5-10 g/100 mL at 20 ºC

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
UB0175000
CHEMICAL NAME :
1-Propanol, 2,3-dibromo-
CAS REGISTRY NUMBER :
96-13-9
BEILSTEIN REFERENCE NO. :
1719127
LAST UPDATED :
199806
DATA ITEMS CITED :
23
MOLECULAR FORMULA :
C3-H6-Br2-O
MOLECULAR WEIGHT :
217.91
WISWESSER LINE NOTATION :
Q1YE1E

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
Standard Draize test
ROUTE OF EXPOSURE :
Administration into the eye
SPECIES OBSERVED :
Rodent - rabbit
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
681 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LC50 - Lethal concentration, 50 percent kill
ROUTE OF EXPOSURE :
Inhalation
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
9920 mg/m3/4H
TOXIC EFFECTS :
Sense Organs and Special Senses (Olfaction) - effect, not otherwise specified Behavioral - somnolence (general depressed activity) Lungs, Thorax, or Respiration - dyspnea
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
125 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rabbit
DOSE/DURATION :
316 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
TCLo - Lowest published toxic concentration
ROUTE OF EXPOSURE :
Inhalation
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
500 mg/m3/4H-3W-I
TOXIC EFFECTS :
Behavioral - somnolence (general depressed activity) Liver - changes in liver weight Related to Chronic Data - death
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
11505 mg/kg/13W-I
TOXIC EFFECTS :
Kidney, Ureter, Bladder - changes in tubules (including acute renal failure, acute tubular necrosis)
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
47940 mg/kg/51W-I
TOXIC EFFECTS :
Tumorigenic - Carcinogenic by RTECS criteria Gastrointestinal - tumors Skin and Appendages - tumors
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
37170 mg/kg/42W-I
TOXIC EFFECTS :
Tumorigenic - Carcinogenic by RTECS criteria Gastrointestinal - tumors Liver - tumors
TYPE OF TEST :
Sex chromosome loss and nondisjunction
TYPE OF TEST :
Heritable translocation test

MUTATION DATA

TYPE OF TEST :
Mutation in mammalian somatic cells
TEST SYSTEM :
Rodent - hamster Lung
DOSE/DURATION :
20 umol/L
REFERENCE :
MUREAV Mutation Research. (Elsevier Science Pub. B.V., POB 211, 1000 AE Amsterdam, Netherlands) V.1- 1964- Volume(issue)/page/year: 124,213,1983

Safety Information

[ Symbol ]:

GHS06, GHS08

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H302 + H332-H311-H350-H361-H412

[ Precautionary Statements ]:
P201-P273-P280-P308 + P313

[ Personal Protective Equipment ]:
Eyeshields;Faceshields;full-face respirator (US);Gloves;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ Hazard Codes ]:
T:Toxic;

[ Risk Phrases ]:
R20/22;R24;R45;R52/53;R62

[ Safety Phrases ]:
S53-S45-S61

[ RIDADR ]:
UN 2810 6.1/PG 2

[ WGK Germany ]:
3

[ RTECS ]:
UB0175000

[ Packaging Group ]:
III

[ Hazard Class ]:
6.1(b)

[ HS Code ]:
2905590090

Synthetic Route

Precursor & DownStream

Precursor

  • Epibromohydrin
  • Allyl alcohol
  • allyl bromide
  • 2,3-dibromopropyl acrylate
  • Glycerol
  • Monopyridin-1-ium tribromide
  • Bromine
  • Water
  • boric acid tris-(2,3-dibromo-propyl ester)

DownStream

  • 2,3-Dihydro-1,4-benzodioxin-2-ylmethanol
  • Allyl alcohol
  • Epibromohydrin
  • Tristealin
  • 2,3-bis(methylsulfanyl)propan-1-ol
  • 1,2-Dimyristoyl-rac-glycerol
  • Glycerol
  • METHYLENE GLYCOL BIS(2,3-DIBROMOPROPYL) ETHER
  • 1-Propanol

Customs

[ HS Code ]: 2905590090

[ Summary ]:
2905590090 other halogenated, sulphonated, nitrated or nitrosated derivatives of acyclic alcohols。Supervision conditions:None。VAT:17.0%。Tax rebate rate:9.0%。MFN tariff:5.5%。General tariff:30.0%

Articles

2-Haloacrylic acids as indicators of mutagenic 2-haloacrolein intermediates in mammalian metabolism of selected promutagens and carcinogens.

J. Agric. Food Chem. 30(4) , 627-31, (1982)

A combination of in vivo selection and cell sorting for the identification of enantioselective biocatalysts.

Angew. Chem. Int. Ed. Engl. 50(37) , 8584-7, (2011)

J. Heterocycl. Chem. 28 , 891, (1991)


More Articles


Related Compounds

  • 2,3-Dibromo-1-propanol hydrogen phosphate ammonium salt
  • 2,3-Dibromo-1,3-bis(4-fluorophenyl)-1-propanone
  • 2,3-dibromo-1-pyridin-4-yl-3-thiophen-2-ylpropan-1-one
  • 2,3-dibromo-1,4-bis-(4-chloro-3-methyl-phenyl)-butane-1,4-dione
  • 2,3-dibromo-1-(5-nitrofuran-2-yl)-3-(2-nitrophenyl)propan-1-one
  • 2,3-dibromo-1,4-dimethoxy-but-2-ene
  • 1-{4-[2-(Dimethyl-1,2-oxazol-4-yl)acetyl]piperazin-1-yl}prop-2-en-1-one
  • 4-((Cyclohexylamino)methyl)benzoic acid hydrochloride
  • 1-[(2,4-Dichlorophenyl)methyl]-N-(1,1-dimethylethyl)-2-methyl-1H-indole-3-methanamine
  • 2-Methoxy-6-(pyrazol-1-yl)-benzonitrile
  • 1H-3-Benzazepin-7-ol, 8-chloro-2,3,4,5-tetrahydro-5-(3-iodophenyl)-3-methyl-, (S)-
  • 4-acetyl-N-{[1-(pyrimidin-2-yl)pyrrolidin-2-yl]methyl}benzene-1-sulfonamide
  • (4-Methyl-tetrahydro-furan-2-yl)-methanol
  • N-(1-cyanocyclopentyl)-2-[4-(4-fluorobenzenesulfonyl)-1,4-diazepan-1-yl]acetamide
  • 5-fluoro-N-[(oxan-4-yl)(thiophen-2-yl)methyl]-1-benzothiophene-2-carboxamide
  • 4,5,6,7-Tetrahydrobenzo[d]isoxazole-3-carbaldehyde