Tributylphosphine

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Names

[ CAS No. ]:
998-40-3

[ Name ]:
Tributylphosphine

[Synonym ]:
Tributylphosphine
EINECS 213-651-2
tri-n-butyl-phosphine
Tris(butyl)phosphine
Phosphine,tributyl
tri-n-butylphosphane
tris(n-butyl)phosphine
UNII:0O52FJR7WN
Tributylfosfin [Czech]
MFCD00009462
Phosphine, tributyl-
Tributylphosphan
Tri-n-Butylphosphine

Chemical & Physical Properties

[ Density]:
0.81 g/mL at 25 °C(lit.)

[ Boiling Point ]:
244.8±0.0 °C at 760 mmHg

[ Melting Point ]:
-65 °C

[ Molecular Formula ]:
C12H27P

[ Molecular Weight ]:
202.316

[ Flash Point ]:
112.2±25.0 °C

[ Exact Mass ]:
202.185043

[ PSA ]:
13.59000

[ LogP ]:
5.60

[ Vapour density ]:
9 (vs air)

[ Vapour Pressure ]:
0.0±0.4 mmHg at 25°C

[ Index of Refraction ]:
n20/D 1.462(lit.)

[ Stability ]:
Stable, but pyrophoric - spontaneously inflammable in air. Incompatible with oxidizing agents. Moisture sensitive.

[ Water Solubility ]:
insoluble

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
SZ3270000
CHEMICAL NAME :
Phosphine, tributyl-
CAS REGISTRY NUMBER :
998-40-3
BEILSTEIN REFERENCE NO. :
1738261
LAST UPDATED :
199701
DATA ITEMS CITED :
3
MOLECULAR FORMULA :
C12-H27-P

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
750 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
34ZIAG "Toxicology of Drugs and Chemicals," Deichmann, W.B., New York, Academic Press, Inc., 1969 Volume(issue)/page/year: -,600,1969
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rabbit
DOSE/DURATION :
2 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
34ZIAG "Toxicology of Drugs and Chemicals," Deichmann, W.B., New York, Academic Press, Inc., 1969 Volume(issue)/page/year: -,600,1969

Safety Information

[ Symbol ]:

GHS02, GHS05, GHS07

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H226-H250-H302-H312-H314

[ Precautionary Statements ]:
P222-P231-P280-P305 + P351 + P338-P310-P422

[ Personal Protective Equipment ]:
Faceshields;full-face respirator (US);Gloves;Goggles;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ Hazard Codes ]:
F:Flammable;C:Corrosive;

[ Risk Phrases ]:
R11;R17;R21/22;R34

[ Safety Phrases ]:
S41-S36/37/39-S26-S16-S45-S43-S17

[ RIDADR ]:
UN 3254 4.2/PG 1

[ WGK Germany ]:
3

[ RTECS ]:
SZ3270000

[ Packaging Group ]:
I

[ Hazard Class ]:
4.2

[ HS Code ]:
2931900090

Synthetic Route

Precursor & DownStream

Precursor

  • Tributylphosphine oxide
  • 1-Bromobutane
  • tributyl(methylthio)phosphonium trifluoromethanesulfonate
  • tri-n-butyl(ethoxycarbonylmethylene)phosphorane
  • Butylmagnesium Bromide
  • carbon monoxide
  • chlorosulfinyloxymethane
  • Cr(CO)5(P(n-Bu)3)
  • TRIBUTYLPHOSPHINE SULFIDE

DownStream

  • 1-(Pyridin-2-yl)piperazin-2-one
  • Tritanol
  • Triphenylmethane
  • 1-[butyl(methyl)phosphoryl]butane
  • Tributylphosphine oxide
  • ac1l3hh9
  • Phosphonium,tributyl(hydroxymethyl)-, chloride (1:1)
  • tributyl(diiodo)-λ5-phosphane

Customs

[ HS Code ]: 2931900090

[ Summary ]:
2931900090. other organo-inorganic compounds. VAT:17.0%. Tax rebate rate:13.0%. Supervision conditions:AB(certificate of inspection for goods inward,certificate of inspection for goods outward). MFN tariff:6.5%. General tariff:30.0%

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Related Compounds

  • CuI(tributylphosphine)
  • Tributylphosphine oxide
  • MeCu(tributylphosphine)
  • tributylphosphine-borane
  • TRIBUTYLPHOSPHINE SULFIDE
  • (tributylphosphine)W(CO)5
  • 1-(7-Chloro-1,3-dioxaindan-5-yl)propan-2-one
  • (4-Propoxythian-4-yl)methanamine
  • rac-(3R,4S)-4-(3-chlorothiophen-2-yl)pyrrolidin-3-ol
  • 3-[2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)hexanamido]-2-methoxypropanoic acid
  • 3,3-Dimethyl-2,6,12-trioxa-9,15-diazadispiro[4.2.5^{8}.2^{5}]pentadecane
  • 9-Ethyl-2,2-dimethyl-5-oxa-8-azaspiro[3.5]nonane
  • 3,3-Difluoro-1-(2-methyloxolan-3-yl)cyclobutan-1-amine
  • 3-Bromo-2-fluoro-4-methylbenzene-1-sulfonyl fluoride
  • 2-(3-Methyloxetan-3-yl)cyclopropan-1-amine
  • 4-amino-1-(2,2-difluorobutyl)-1H-pyrazole-3-carboxamide
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