Journal of Organic Chemistry 2007-03-16

Regio- and stereospecific synthesis of beta-sulfonamidodisulfides and beta-sulfonamidosulfides from aziridines using tetrathiomolybdate as a sulfur transfer reagent.

Devarajulu Sureshkumar, Thanikachalam Gunasundari, Venkataraman Ganesh, Srinivasan Chandrasekaran

文献索引：J. Org. Chem. 72 , 2106, (2007)

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摘要

A comprehensive study of a general and effective one-step procedure for the synthesis of beta-sulfonamidodisulfides directly from N-tosyl aziridines in a regio- and stereospecific manner under neutral conditions without the use of any Lewis acid or base has been reported. This methodology is extended to the synthesis of an optically pure cyclic seven-membered disulfide 29. Synthesis of a variety of beta-sulfonamidosulfides involving tandem, multistep reactions in one pot is also reported.

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  • 四硫钼酸铵

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