Journal of Chromatography A 2006-01-01

A new silylating reagent–dimethyl(3,3,3-trifluoropropyl)silyldiethylamine–for the derivatisation of non-steroidal anti-inflammatory drugs prior to gas chromatography-mass spectrometry analysis

Magda Caban, Katarzyna Mioduszewska, Paulina Łukaszewicz, Natalia Migowska, Piotr Stepnowski, Marek Kwiatkowski, Jolanta Kumirska

文献索引:J. Chromatogr. A. 1346 , 107-16, (2014)

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摘要

• DIMETRIS–a new silylating reagent for the derivatisation of NSAIDs. • Derivatising properties of DIMETRIS compared with those of BSTFA and TMSD. • Possibility of using MS and ECD detectors for the GC determination of new derivatives. • Study of the influence of complex matrices on derivatisation and GC-MS analysis. • A new SPE-GC-MS method for determining NSAIDs based on derivatisation with DIMETRIS


相关化合物

  • 正己烷
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  • 异丙甲草胺 草酸盐
  • N,O-双(三甲基硅烷...
  • 2-甲基蒽
  • 氯二甲基-3,3,3-氟...

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