Molecules 2011-01-01

Facile preparation of the tosylhydrazone derivatives of a series of racemic trans-3,4-substituted cyclopentanones.

Kamal H Bouhadir, Bilal Abou Aleiwe, Fares A Fares

文献索引：Molecules 17(1) , 1-14, (2011)

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摘要

We report the synthesis and characterization of a variety of trans-3,4-substituted cyclopentanones and the corresponding tosylhydrazone derivatives starting with diethyl fumarate. Protection of the keto group followed by selective monohydrolysis of esters was achieved, resulting in cyclopentanones with different substituents at positions 3 and 4. The tosylhydrazone derivative of each cyclopentanone intermediate was prepared in moderate to good yields. These compounds are potential precursors for functionalized methanofullerenes.

相关化合物

  • 环戊酮
  • 富马酸二乙酯

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