International Journal of Radiation Applications and Instrumentation. Part A. Applied Radiation and Isotopes 1986-01-01

Synthesis and identification of [76As]arsenic trichloride.

A M Emran, N M Shanbaky, R P Spencer

文献索引：Int. J. Rad. Appl. Instrum. A. 37(6) , 545-7, (1986)

全文：HTML全文

摘要

Radiosynthesis of arsenic trichloride (AsCl3) was achieved using 76As as the radionuclide of choice for preliminary investigations. The synthesis required neutron activation of arsenic trioxide (As2O3) followed by reaction with sulfur monochloride (S2Cl2) under a dry inert atmosphere. The synthesized 76AsCl3 was purified by distillation or partially purified by treatment with dry acetonitrile followed by filtration. Identification was accomplished by thin layer chromatography (TLC) and reversed phase high performance liquid chromatography (HPLC). 76AsCl3 was used for synthesis of a dihydrophenarsazine derivative.

相关化合物

  • 三氯化砷

相关文献：

Remediation of mercury contaminated saltwater with functionalized silica coated magnetite nanoparticles.

2016-07-01

[Sci. Total Environ. 557-558 , 712-21, (2016)]

[Anti-apoptosis effect of VEGF on the human chronic myelocytic leukemia cell line K562].

2005-10-01

[Zhongguo Shi Yan Xue Ye Xue Za Zhi 13(5) , 778-82, (2005)]

Mechanism of action of all-trans retinoic acid and arsenic trioxide in the treatment of acute promyelocytic leukemia.

2002-02-01

[Gan To Kagaku Ryoho. 29 Suppl 1 , 214-8, (2002)]

Caspase-independent cell death by arsenic trioxide in human cervical cancer cells: reactive oxygen species-mediated poly(ADP-ribose) polymerase-1 activation signals apoptosis-inducing factor release from mitochondria.

2004-12-15

[Cancer Res. 64(24) , 8960-7, (2004)]

Nucleolin links to arsenic-induced stabilization of GADD45alpha mRNA.

2006-01-01

[Nucleic Acids Res. 34(2) , 485-95, (2006)]

更多文献...