Journal of Combinatorial Chemistry
2002-01-01
Solid-phase synthesis of n,n-disubstituted s,n'-diarylisothioureas: facile exchange reactions of isocyanates.
Alan R Katritzky, Vladimir Vvedensky, Boris V Rogovoy, Katherine Kovalenko, Eduardo Torres, Behrouz Forood
文献索引:J. Comb. Chem. 4(4) , 285-9, (2002)
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摘要
Reactions of resin-bound 1,1-disubstituted-2-arylisothioureas 4aa',ab'-ec' with aryl isocyanates, diversely substituted at the para and/or meta positions, and with o-fluoro- and 2,4-difluorophenyl isocyanate followed by appropriate cleavage led to the formation of N,N-disubstituted S,N'-diarylisothioureas 9[1-70] in good yields and high purities.
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