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1,2-萘醌-4-磺酸钠盐

1,2-萘醌-4-磺酸钠盐用途

1.用作薄层色谱和纸色谱法测定氨基酸的显色剂。还用作染料中间体。

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1,2-萘醌-4-磺酸钠盐名称

[ CAS 号 ]:
521-24-4

[ 中文名 ]:
1,2-萘醌-4-磺酸钠

[ 英文名 ]:
Folin's reagent

[中文别名 ]:

[英文别名 ]:

Sodium 1,2-Naphthoquinone-4-sulfonate
EINECS 208-308-9
MFCD00001700
Folin's reagent
1,2-Naphthoquinone-4-sulfonic Acid Sodium Salt
sodium,3,4-dioxonaphthalene-1-sulfonate

1,2-萘醌-4-磺酸钠盐物理化学性质

[ 熔点 ]:
289 °C (dec.)(lit.)

[ 分子式 ]:
C₁₀H₅NaO₅S

[ 分子量 ]:
260.198

[ 精确质量 ]:
259.975525

[ PSA ]:
99.72000

[ LogP ]:
1.41890

[ 外观性状 ]:
粉末

[ 储存条件 ]:
2-8°C

[ 稳定性 ]:
Stable. Incompatible with strong oxidizing agents.

[ 水溶解性 ]:
H2O: 50 mg/mL, clear

1,2-萘醌-4-磺酸钠盐MSDS

详细MSDS(安全技术说明书)

1,2-萘醌-4-磺酸钠盐毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: QK1490000

CHEMICAL NAME :: 1-Naphthalenesulfonic acid, 3,4-dihydro-3,4-dioxo-, sodium salt

CAS REGISTRY NUMBER :: 521-24-4

LAST UPDATED :: 199701

DATA ITEMS CITED :: 3

MOLECULAR FORMULA :: C10-H6-O5-S.Na

MOLECULAR WEIGHT :: 261.21

WISWESSER LINE NOTATION :: L66 BVVJ ESWQ &-NA-

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Intraperitoneal

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 625 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: NTIS** National Technical Information Service. (Springfield, VA 22161) Formerly U.S. Clearinghouse for Scientific & Technical Information. Volume(issue)/page/year: AD691-490 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - X7927 No. of Facilities: 25 (estimated) No. of Industries: 1 No. of Occupations: 1 No. of Employees: 1358 (estimated) No. of Female Employees: 956 (estimated)

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1,2-萘醌-4-磺酸钠盐安全信息

[ 个人防护装备 ]:
dust mask type N95 (US);Eyeshields;Gloves

[ 危害码 (欧洲) ]:
Xi: Irritant;

[ 风险声明 (欧洲) ]:
R36/37/38

[ 安全声明 (欧洲) ]:
S26

[ 危险品运输编码 ]:
NONH for all modes of transport

[ WGK德国 ]:
3

[ RTECS号 ]:
QK1490000

[ 海关编码 ]:
2914399090

1,2-萘醌-4-磺酸钠盐上下游产品

1,2-萘醌-4-磺酸钠盐上游产品

1,2-萘醌-4-磺酸钠盐下游产品

1,2-萘醌-4-磺酸钠盐制备

1.不断搅拌下，将无水无色的１-氨基-２-萘酚-４-磺酸分次少量加到已冷至30℃的20%的稀硝酸中，每次加料必须充分搅拌，必要时可加适量乙醚消泡，并控制反应温度在20～25℃，加料结束后，将温度降至5～10℃，然后加入30℃的饱和氯化铵溶液，继续冷却至0℃，静置后过滤，结晶用少量冰冷的稀氯化铵溶液洗涤三次，再用乙醇洗涤二次，用乙醚洗涤数次，所得１-2-萘醌-４-磺酸在35～40℃干燥至恒重。然后用50℃的水溶解干燥的1-２-萘醌-４- 磺酸，加活性炭脱色。将30℃
的饱和氯化钠溶液加到过滤后的澄清桔色滤液中，静置冷却至０℃，滤出的结晶依次用稀氯化钠冷溶液、乙醇、乙醚洗涤至合格，并干燥至恒重，即得1,2-萘醌-４-磺酸钠。
过程主要反应为：

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1,2-萘醌-4-磺酸钠盐海关

[ 海关编码 ]: 2914399090

[ 中文概述 ]:
2914399090. 其他不含其他含氧基的芳香酮. 增值税率:17.0%. 退税率:13.0%. 监管条件:无. 最惠国关税:5.5%. 普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 丙酮报明包装

[ Summary ]:
2914399090. other aromatic ketones without other oxygen function. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:5.5%. General tariff:30.0%

1,2-萘醌-4-磺酸钠盐文献

A histochemical examination of the staining of kainate-induced neuronal degeneration by anionic dyes.

Biotech. Histochem. 73(5) , 244-54, (1998)

Anionic dyes, notably acid fuchsine, strongly stain the nuclei and cytoplasm of neurons severely damaged by injury or disease. We provide detailed instructions for staining nervous tissue with toluidi...

Spectrophotometric determination of aminomethylbenzoic acid using sodium 1,2-naphthoquinone-4-sulfonate as the chemical derivative chromogenic reagent.

Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 66(3) , 656-61, (2007)

A new method has been established for the determination of aminomethylbenzoic acid using sodium 1,2-naphthoquinone-4-sulfonate as the chemical derivative chromogenic reagent. This method is based on t...

Spectophotometric methods for determination of cefdinir in pharmaceutical formulations via derivatization with 1,2-naphthoquinone-4-sulfonate and 4-chloro-7-nitrobenzo-2-oxa-1, 3-diazole.

Drug Test. Anal. 4(12) , 991-1000, (2012)

Two new simple, sensitive, accurate, and precise spectrophotometric methods have been developed and validated for the determination of cefdinir (CFD) in bulk drug and in its pharmaceutical formulation...

更多文献

1,2-萘醌-4-磺酸钠盐

1,2-萘醌-4-磺酸钠盐用途

1,2-萘醌-4-磺酸钠盐名称

1,2-萘醌-4-磺酸钠盐物理化学性质

1,2-萘醌-4-磺酸钠盐MSDS

详细MSDS(安全技术说明书)

1,2-萘醌-4-磺酸钠盐毒性和生态

CHEMICAL IDENTIFICATION

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

1,2-萘醌-4-磺酸钠盐安全信息

1,2-萘醌-4-磺酸钠盐上下游产品

1,2-萘醌-4-磺酸钠盐上游产品

1,2-萘醌-4-磺酸钠盐下游产品

1,2-萘醌-4-磺酸钠盐制备

1,2-萘醌-4-磺酸钠盐海关

1,2-萘醌-4-磺酸钠盐文献

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