The use of Bunte salts in synthesis. I. The preparation of mercaptals

HE Westlake Jr, G Dougherty

文献索引：Westlake; Dougherty Journal of the American Chemical Society, 1941 , vol. 63, p. 659

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被引用次数: 26

摘要

The ether was evaporated under reduced pressure and the sirupy residue taken up in alcohol. A small amount of amorphous solid separated and was removed by filtration. The alcoholic solution was poured into ether and the re- sulting solution washed thoroughly with water and then ex- tracted with 5% sodium carbonate solution. The in- tensely red aqueous layer was separated and acidiiled and extracted with ether. The ether layer was washed with several portions ...