V. To a well-stirred solution of 73 g (0.35 mol) of IV in 750 mL of CH2C12 at room temperature under N2 was added a slurry of 72 g (0.37 mol, 85% quality) of m- chloroperbenzoic acid in 700 mL of CH2C12. The reaction was slightly exothermic and was maintained below 35" C with a water bath. After 2 h the reaction was judged complete by TLC, and the volume was reduced to 500 mL in vacuo. Upon dilution with an equal ...
![[2-(2-氟-3,4-二甲氧基)苯基]乙胺结构式](https://image.chemsrc.com/caspic/043/72912-24-4.png)
