Preparation and synthetic utility of phase-transfer catalysts anchored to polystyrene

MS Chiles, DD Jackson, PC Reeves

文献索引：Chiles, Margaret Shea; Jackson, Donald D.; Reeves, Perry C. Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2915 - 2918

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被引用次数: 53

摘要

Org. Chem. 1978, 43, 4509. mL of 50% tert-butyl alcohol-doubly distilled water was added sodium hydroxide (1.517 g, 38 mmol), and the system was degassed and then constantly swept with nitrogen free of oxygen, under magnetic stirring. This was followed by the addition of bromobenzene (1 mL, 9.5 mmol) and toluene (0.5 mL) as internal standard. A 2- mL aliquot was removed at different reaction times to check the toluene/bromobenzene ...