Abstract Phenyl phosphorodichloridate (1) is readily prepared by reaction of phenol with phosphoryl chloride at low temperature. The crude product is white in colour is subjected to vacuum distillation. However, this reagent reacts only poorly with bis (2-chloroethyl) amine hydrochloride at ambient temperature; thus, an alternative route was sought to aniline and to give 2 and 3, respectively compounds. Compound (3) reacted with aniline and ...
[Orji, Charles C.; Pinkus, A. G. Organic Preparations and Procedures International, 1994 , vol. 26, # 6 p. 691 - 695 Title/Abstract Full Text Show Details Orji, C. C.; Reibenspies, J. H.; Meyers, E. A.; Pinkus, A. G. Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 97, # 1-4 p. 9 - 16]
