Copper-mediated radical trifluoromethylation of unsaturated potassium organotrifluoroborates

M Presset, D Oehlrich, F Rombouts…

文献索引：Journal of Organic Chemistry, , vol. 78, # 24 p. 12837 - 12843

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被引用次数: 33

摘要

... The Journal of Organic ... 1 H NMR (400 MHz/DMSO-d 6 ): δ 7.66 (d, J = 7 Hz, 2H), 7.59 (d, J = 8 Hz, 2H), 7.46 (dd, J = 8, 8 Hz, 2H), 7.40–7.33 (m, 3H). ... The combined organic layers were washed with brine (50 mL), dried (MgSO 4 ), and evaporated to afford the crude product. ...