Tetrahedron

Direct oxidative conversion of alkyl halides into nitriles with molecular iodine and 1, 3-diiodo-5, 5-dimethylhydantoin in aq ammonia

S Iida, R Ohmura, H Togo

文献索引：Iida, Shinpei; Ohmura, Ryosuke; Togo, Hideo Tetrahedron, 2009 , vol. 65, # 31 p. 6257 - 6262

被引用次数: 48

摘要

Various benzylic halides were smoothly and directly converted into the corresponding aromatic nitriles in high yields using molecular iodine and 1, 3-diiodo-5, 5- dimethylhydantoin, respectively, in aq ammonia. Similarly, primary alkyl halides were also converted into corresponding nitriles in moderate to good yields using molecular iodine and 1, 3-diiodo-5, 5-dimethylhydantoin in aq ammonia, although a long reaction time was ...

~61%

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~49%

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~77%

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~82%

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~86%

2571-52-0

2,4,6-三甲基苯甲腈

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~85%

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~90%

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~66%

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~58%

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~61%

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~39%

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~68%

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~57%

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~71%

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~75%

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~63%

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~48%

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~76%

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~67%

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~49%

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~83%

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~75%

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