From adenosine to 3'-deoxyadenosine: development and scale up

S Aman, DJ Anderson, TJ Connolly…

文献索引：Schirmeister-Tichy, Helga; Iacono, Kathryn T.; Muto, Nicholas F.; Homan, Joseph W.; Suhadolnik, Robert J.; Pfleiderer, Wolfgang Helvetica Chimica Acta, 1999 , vol. 82, # 4 p. 597 - 613

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被引用次数: 28

摘要

... It was also discovered during the stage one development that the reaction worked better in a 50/50 (w/w) mixture of acetonitrile/ethyl acetate, and ... dd, J = 12.5, 6.0 Hz, 1H), 3.81 (dd, J = 12.5, 6.0 Hz, 1H), 4.40 (q, J = 6.0 Hz 1H), 4.59 (dd, J = 6.0, 3.5 Hz, 1H), 4.78 (t, J = 3.5 Hz ...