Observations on the deprotection of pinanediol and pinacol boronate esters via fluorinated intermediates

SR Inglis, ECY Woon, AL Thompson…

Index: Al-Juaid, Salih S.; Eaborn, Colin; El-Kheli, Mohamed N. A.; Hitchcock, Peter R.; Lickiss, Paul D.; et al. Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 447 - 452

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Citation Number: 23

Abstract

... acids in tris(hydroxymethyl)aminomethane (tris) buffer.(10) Studies on difluoroborane 15 in D 2 O/CD ... was consistent with that of an original enantiopure sample of 9 (Scheme S-1, Supporting ... with ethyl acetate; the combined extracts were washed with brine and dried (Na 2 SO 4 ...