Synthetic Communications®

New Deoxygenation Method for Amine N-Oxides Using Dimethylthiocarbamoyl Chloride

H Caliskan, Ö Zaim

Index: Caliskan, Hafize; Zaim, Oemer Synthetic Communications, 2010 , vol. 40, # 20 p. 3078 - 3083

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Abstract

View all references ] A number of methods have been described for the reduction of amine N-oxides, including agents such as low-valent titanium, [ 2 2. (a) Malinowski , M. Titanium(0) reagents, 1: A facile deoxygenation of unfunctionalized aromatic N-oxides . Synthesis 1987 , 732 – 734 ; (b) Balicki , R. TiCl4/NaI: A novel, efficient reagent for mild reduction of the NO bond in amine N-oxides and nitrones . Chem. Ber. 1990 , 647 – 648 ; (c) Balicki , R. ; ...

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