Inert carbon free radicals. 5. Perchloro-9-phenylfluorenyl radical series

M Ballester, J Castañer, J Riera, J Pujadas…

Index: Ballester, M.; Castaner, J.; Riera, J.; Pujadas, J.; Armet, O.; et al. Journal of Organic Chemistry, 1984 , vol. 49, p. 770 - 778

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Citation Number: 15

Abstract

The synthesis of the perchloro-9-phenylfluorenyl radical (PPF) from 9-phenylfluorene (1) has been accomplished through a chlorolytic aromatic perchlorination to aH-pentadecachloro-2- biphenylylphenylmethane(2) with BMC reagent, followed by a cyclization at 300 “C (91%). The radical PPF is also obtained by cyclization at 320 “C of the perchlorotriphenylmethyl radical (PTM). Other syntheses of the radical PPF are described. PPF is chlorinated to ...

 Related Synthetic Route
αH-Pentadecachloro-2-biphenylylphenylmethane Structure

88180-04-5

αH-Pentadecachl...

~92%

1,2,3,4,5,6,7,8-octachloro-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-05-6

1,2,3,4,5,6,7,8...

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1,2,3,4,5,6,7,8-Octachloro-9-(pentachlorophenyl)-9H-fluoren-9-ylradical Structure

32390-14-0

1,2,3,4,5,6,7,8...

~66%

1,2,3,4,5,6,7,8-octachloro-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-05-6

1,2,3,4,5,6,7,8...

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1,2,3,4,5,6,7,8-Octachloro-9-(pentachlorophenyl)-9H-fluoren-9-ylradical Structure

32390-14-0

1,2,3,4,5,6,7,8...

~78%

1,2,3,4,5,6,7,8,9-nonachloro-9-(2,3,4,5,6-pentachlorophenyl)fluorene Structure

88180-06-7

1,2,3,4,5,6,7,8...

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3-Methoxydodecachloro-9-phenylfluorenyl radical Structure

88180-09-0

3-Methoxydodeca...

~90%

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

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αH-Pentadecachloro-2-biphenylylphenylmethane Structure

88180-04-5

αH-Pentadecachl...

~81%

1,2,3,4,5,6,7,8-Octachloro-9-(pentachlorophenyl)-9H-fluoren-9-ylradical Structure

32390-14-0

1,2,3,4,5,6,7,8...

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

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1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluoren-3-ol Structure

88180-10-3

1,2,4,5,6,7,8-h...

~%

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

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9H-Dodecachloro-3-methoxy-9-phenylfluorene Structure

88180-12-5

9H-Dodecachloro...

~%

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

Learn More
1,2,3,4,5,6,7,8-Octachloro-9-(pentachlorophenyl)-9H-fluoren-9-ylradical Structure

32390-14-0

1,2,3,4,5,6,7,8...

~26%

Perchloro-4-(9-fluorenylidene)cyclohexa-2,5-dienone Structure

88180-08-9

Perchloro-4-(9-...

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

Learn More
9H-3-Acetoxydodecachloro-9-phenylfluorene Structure

88180-11-4

9H-3-Acetoxydod...

~%

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

Learn More
perchloro(diphenylmethylene)cyclohexa-2,5-dienone Structure

29972-98-3

perchloro(diphe...

~26%

Perchloro-4-(9-fluorenylidene)cyclohexa-2,5-dienone Structure

88180-08-9

Perchloro-4-(9-...

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

Learn More
1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)fluoren-3-one Structure

88180-07-8

1,2,4,5,6,7,8-h...

~75%

1,2,4,5,6,7,8-heptachloro-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluoren-3-ol Structure

88180-10-3

1,2,4,5,6,7,8-h...

Learn More
Hexachlorobenzene Structure

118-74-1

Hexachlorobenzene

3-methylfluoren-9-one Structure

1705-89-1

3-methylfluoren...

~%

3-methyl-9-(2,3,4,5,6-pentachlorophenyl)fluoren-9-ol Structure

88180-15-8

3-methyl-9-(2,3...

Learn More
3-methyl-9-(2,3,4,5,6-pentachlorophenyl)fluoren-9-ol Structure

88180-15-8

3-methyl-9-(2,3...

~93%

3-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-16-9

3-methyl-9-(2,3...

Learn More
Hexachlorobenzene Structure

118-74-1

Hexachlorobenzene

~%

3-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-16-9

3-methyl-9-(2,3...

Learn More
3-methylfluoren-9-one Structure

1705-89-1

3-methylfluoren...

~%

3-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-16-9

3-methyl-9-(2,3...

Learn More
3-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-16-9

3-methyl-9-(2,3...

~64%

1,2,3,4,5,7,8-heptachloro-6-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-17-0

1,2,3,4,5,7,8-h...

Learn More
Hexachlorobenzene Structure

118-74-1

Hexachlorobenzene

~%

1,2,3,4,5,7,8-heptachloro-6-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-17-0

1,2,3,4,5,7,8-h...

Learn More
3-methylfluoren-9-one Structure

1705-89-1

3-methylfluoren...

~%

1,2,3,4,5,7,8-heptachloro-6-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-17-0

1,2,3,4,5,7,8-h...

Learn More
3-methyl-9-(2,3,4,5,6-pentachlorophenyl)fluoren-9-ol Structure

88180-15-8

3-methyl-9-(2,3...

~%

1,2,3,4,5,7,8-heptachloro-6-methyl-9-(2,3,4,5,6-pentachlorophenyl)-9H-fluorene Structure

88180-17-0

1,2,3,4,5,7,8-h...

Learn More
9-(2-phenylphenyl)fluoren-9-ol Structure

67665-44-5

9-(2-phenylphen...

~78%

9-(2-phenylphenyl)-9H-fluorene Structure

88180-19-2

9-(2-phenylphen...

Learn More

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