The Journal of Organic Chemistry

Stereoselective Preparation of Deuterium-Labeled Sugars:(6 R)-(6-2H1)-N-Acetylglucosamine Derivatives

ML Falcone-Hindley, JT Davis

Index: Journal of Organic Chemistry, , vol. 63, # 16 p. 5555 - 5561

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Citation Number: 9

Abstract

... The Journal of Organic ... 4b,5a Recent ROESY experiments in an organic solvent revealed that glycopeptide Ac-Asn(β1-N-GlcNAc)Leu-Thr-NH 2 (1) had peptide−sugar NOEs ... of a single deuterium into the C6 position of 7α-d was confirmed by 1 H, 2 H, and 13 C (J CD = 21.8 Hz ...