Journal of the American Chemical Society

Organoboron Compounds. IV. 1 Aminoethyl Diarylborinates

RL Letsinger, I Skoog

Index: Letsinger; Skoog Journal of the American Chemical Society, 1955 , vol. 77, p. 2491,2492,2494

Full Text: HTML

Citation Number: 67

Abstract

A practical procedure has been developed for the preparation of aminoethyl diphenylborinate. This involves the reaction of phenylmagnesium bromide with butyl borate at low temperature, isolation of butyl diphenylborinate as a complex with ammonia, and conversion of the ammonia complex to the aminoethyl ester with ethanolamine. Aminoethyl bis-(p-bromophenyl)-borinate was prepared by similar techniques. Solid derivatives of ...