New synthetic methods. Conjugate addition of alkyl groups to electron deficient olefins with nitroalkanes as alkyl anion equivalents

…, A Kamimura, H Miyake, I Hamamoto…

Index: Ono, Noboru; Kamimura, Akio; Miyake, Hideyoshi; Hamamoto, Isami; Kaji, Aritsune Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3692 - 3698

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Citation Number: 80

Abstract

Fluorescence Measurements. The steady-state fluorescence measurements were performed in a right-angle geometry with a spectrofluorimeter from SLM; a description of this apparatus has been given in a previous publication.20 Laser Flash Photolysis. For laser flash photolysis, excitation was carried out in a front-face configuration with 337.1-nm laser pulses (8 ns, 2-3 mJ) from a Molectron UV-400 system or 425-nm laser pulses (6 ns, 2-10 mJ), ...