Liebigs Annalen der Chemie

Polyine, 3. Synthese von (1, 3??Alkadiinyl) aminen

M Feustel, G Himbert

Index: Feustel, Michael; Himbert, Gerhard Liebigs Annalen der Chemie, 1984 , # 3 p. 586 - 599

Full Text: HTML

Citation Number: 6

Abstract

Abstract Durch Umsetzung von (3, 4, 4-Trichlor-3-buten-1-inyl) aminen 2 oder (Pentachlor-1, 3-butadienyl)-aminen 4 mit der zweifach bzw. dreifach äquimolaren Menge Butyllithium werden die entsprechenden Lithium-(4-amino-1, 3-butadiinide) 5 erzeugt. Diese liefern nach Umsetzung mit Wasser, Alkyliodiden, Chlorameisensäureester und Elementhalogeniden oder mit Ketonen, Kohlendioxid, Isocyanaten, Isothiocyanaten und ...

 Related Synthetic Route
4-(3,4,4-trichlorobut-3-en-1-ynyl)morpholine Structure

60014-60-0

4-(3,4,4-trichl...

~%

lithium,4-buta-1,3-diynylmorpholine Structure

80487-51-0

lithium,4-buta-...

Learn More
4-(3,4,4-trichlorobut-3-en-1-ynyl)morpholine Structure

60014-60-0

4-(3,4,4-trichl...

~%

trimethyl(4-morpholin-4-ylbuta-1,3-diynyl)silane Structure

82505-78-0

trimethyl(4-mor...

Learn More
Chlorotrimethylsilane Structure

75-77-4

Chlorotrimethyl...

lithium,4-buta-1,3-diynylmorpholine Structure

80487-51-0

lithium,4-buta-...

~43%

trimethyl(4-morpholin-4-ylbuta-1,3-diynyl)silane Structure

82505-78-0

trimethyl(4-mor...

Learn More
4-(3,4,4-trichlorobut-3-en-1-ynyl)morpholine Structure

60014-60-0

4-(3,4,4-trichl...

~%

trimethyl(4-morpholin-4-ylbuta-1,3-diynyl)stannane Structure

82505-79-1

trimethyl(4-mor...

Learn More
Trimethyltin chloride Structure

1066-45-1

Trimethyltin ch...

lithium,4-buta-1,3-diynylmorpholine Structure

80487-51-0

lithium,4-buta-...

~20%

trimethyl(4-morpholin-4-ylbuta-1,3-diynyl)stannane Structure

82505-79-1

trimethyl(4-mor...

Learn More
N-(4-diphenylphosphanylbuta-1,3-diynyl)-N-methylaniline Structure

82505-84-8

N-(4-diphenylph...

~64%

N-(4-diphenylphosphorylbuta-1,3-diynyl)-N-methylaniline Structure

90235-51-1

N-(4-diphenylph...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-(4-diphenylphosphorylbuta-1,3-diynyl)-N-methylaniline Structure

90235-51-1

N-(4-diphenylph...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~%

N-(4-diphenylphosphorylbuta-1,3-diynyl)-N-methylaniline Structure

90235-51-1

N-(4-diphenylph...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~54%

N-buta-1,3-diynyl-N-methylaniline Structure

82505-80-4

N-buta-1,3-diyn...

Learn More
Triphenylgermanium bromide, 95% Structure

3005-32-1

Triphenylgerman...

((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~64%

N-methyl-N-(4-triphenylgermylbuta-1,3-diynyl)aniline Structure

82505-82-6

N-methyl-N-(4-t...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-methyl-N-(4-triphenylgermylbuta-1,3-diynyl)aniline Structure

82505-82-6

N-methyl-N-(4-t...

Learn More
diphenyl chloroarsine Structure

712-48-1

diphenyl chloro...

N-methyl-N-(4-trimethylstannylbuta-1,3-diynyl)aniline Structure

82505-83-7

N-methyl-N-(4-t...

~74%

N-(4-diphenylarsanylbuta-1,3-diynyl)-N-methylaniline Structure

90235-52-2

N-(4-diphenylar...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-(4-diphenylarsanylbuta-1,3-diynyl)-N-methylaniline Structure

90235-52-2

N-(4-diphenylar...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~%

N-(4-diphenylarsanylbuta-1,3-diynyl)-N-methylaniline Structure

90235-52-2

N-(4-diphenylar...

Learn More
4-(3,4,4-trichlorobut-3-en-1-ynyl)morpholine Structure

60014-60-0

4-(3,4,4-trichl...

~%

1-(4-morpholin-4-ylbuta-1,3-diynyl)cyclododecan-1-ol Structure

90235-53-3

1-(4-morpholin-...

Learn More
lithium,4-buta-1,3-diynylmorpholine Structure

80487-51-0

lithium,4-buta-...

Cyclododecanone Structure

830-13-7

Cyclododecanone

~40%

1-(4-morpholin-4-ylbuta-1,3-diynyl)cyclododecan-1-ol Structure

90235-53-3

1-(4-morpholin-...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

Cyclododecanone Structure

830-13-7

Cyclododecanone

~95%

1-[4-(N-methylanilino)buta-1,3-diynyl]cyclododecan-1-ol Structure

90235-54-4

1-[4-(N-methyla...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

1-[4-(N-methylanilino)buta-1,3-diynyl]cyclododecan-1-ol Structure

90235-54-4

1-[4-(N-methyla...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-methyl-N-(4-trimethylstannylbuta-1,3-diynyl)aniline Structure

82505-83-7

N-methyl-N-(4-t...

Learn More
Trimethyltin chloride Structure

1066-45-1

Trimethyltin ch...

((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~44%

N-methyl-N-(4-trimethylstannylbuta-1,3-diynyl)aniline Structure

82505-83-7

N-methyl-N-(4-t...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

Chlorodiphenylphosphine Structure

1079-66-9

Chlorodiphenylp...

~48%

N-(4-diphenylphosphanylbuta-1,3-diynyl)-N-methylaniline Structure

82505-84-8

N-(4-diphenylph...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-(4-diphenylphosphanylbuta-1,3-diynyl)-N-methylaniline Structure

82505-84-8

N-(4-diphenylph...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

methyl 5-(N-methylanilino)penta-2,4-diynoate Structure

82505-85-9

methyl 5-(N-met...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

Methyl chloroformate Structure

79-22-1

Methyl chloroformate

~39%

methyl 5-(N-methylanilino)penta-2,4-diynoate Structure

82505-85-9

methyl 5-(N-met...

Learn More
Cyclohexanone Structure

108-94-1

Cyclohexanone

((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~71%

1-[4-(N-methylanilino)buta-1,3-diynyl]cyclohexan-1-ol Structure

90235-55-5

1-[4-(N-methyla...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

1-[4-(N-methylanilino)buta-1,3-diynyl]cyclohexan-1-ol Structure

90235-55-5

1-[4-(N-methyla...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

Cyclopentanone Structure

120-92-3

Cyclopentanone

~59%

1-[4-(N-methylanilino)buta-1,3-diynyl]cyclopentan-1-ol Structure

90235-56-6

1-[4-(N-methyla...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

1-[4-(N-methylanilino)buta-1,3-diynyl]cyclopentan-1-ol Structure

90235-56-6

1-[4-(N-methyla...

Learn More
N-(4-diphenylphosphanylbuta-1,3-diynyl)-N-methylaniline Structure

82505-84-8

N-(4-diphenylph...

~74%

N-(4-diphenylphosphinothioylbuta-1,3-diynyl)-N-methylaniline Structure

90250-74-1

N-(4-diphenylph...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-(4-diphenylphosphinothioylbuta-1,3-diynyl)-N-methylaniline Structure

90250-74-1

N-(4-diphenylph...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~%

N-(4-diphenylphosphinothioylbuta-1,3-diynyl)-N-methylaniline Structure

90250-74-1

N-(4-diphenylph...

Learn More
4-(3,4,4-trichlorobut-3-en-1-ynyl)morpholine Structure

60014-60-0

4-(3,4,4-trichl...

~%

4-hexa-1,3-diynylmorpholine Structure

90235-42-0

4-hexa-1,3-diyn...

Learn More
lithium,4-buta-1,3-diynylmorpholine Structure

80487-51-0

lithium,4-buta-...

Ethyl iodide Structure

75-03-6

Ethyl iodide

~3%

4-hexa-1,3-diynylmorpholine Structure

90235-42-0

4-hexa-1,3-diyn...

Learn More
Piperidine Structure

110-89-4

Piperidine

~%

trimethyl(4-piperidin-1-ylbuta-1,3-diynyl)silane Structure

90235-44-2

trimethyl(4-pip...

Learn More
Chlorotrimethylsilane Structure

75-77-4

Chlorotrimethyl...

N-Pentachlor-1,3-butadienyl-piperidin Structure

13178-30-8

N-Pentachlor-1,...

~%

1,4-BIS(TRIMETHYLSILYL)-1,3-BUTADIYNE Structure

4526-07-2

1,4-BIS(TRIMETH...

trimethyl(4-piperidin-1-ylbuta-1,3-diynyl)silane Structure

90235-44-2

trimethyl(4-pip...

Learn More
lithium N,N-diphenylamide Structure

5856-89-3

lithium N,N-dip...

~%

5-(N-phenylanilino)penta-2,4-diynoic acid Structure

90235-57-7

5-(N-phenylanil...

Learn More
N-phenyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-77-9

N-phenyl-N-(3,4...

~%

5-(N-phenylanilino)penta-2,4-diynoic acid Structure

90235-57-7

5-(N-phenylanil...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

tert-Butylisocyanate Structure

1609-86-5

tert-Butylisocyanate

~44%

N-tert-butyl-5-(N-methylanilino)penta-2,4-diynamide Structure

90235-58-8

N-tert-butyl-5-...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-tert-butyl-5-(N-methylanilino)penta-2,4-diynamide Structure

90235-58-8

N-tert-butyl-5-...

Learn More
N-phenyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-77-9

N-phenyl-N-(3,4...

~%

N-tert-butyl-5-(N-phenylanilino)penta-2,4-diynamide Structure

82505-86-0

N-tert-butyl-5-...

Learn More
Chlorotrimethylsilane Structure

75-77-4

Chlorotrimethyl...

((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~61%

N-methyl-N-(4-trimethylsilylbuta-1,3-diynyl)aniline Structure

90235-45-3

N-methyl-N-(4-t...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-methyl-N-(4-trimethylsilylbuta-1,3-diynyl)aniline Structure

90235-45-3

N-methyl-N-(4-t...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

Cyclohexyl Isothiocyanate Structure

1122-82-3

Cyclohexyl Isot...

~46%

N-cyclohexyl-5-(N-methylanilino)penta-2,4-diynethioamide Structure

90235-59-9

N-cyclohexyl-5-...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-cyclohexyl-5-(N-methylanilino)penta-2,4-diynethioamide Structure

90235-59-9

N-cyclohexyl-5-...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-methyl-N-(4-methylsulfanylbuta-1,3-diynyl)aniline Structure

90235-61-3

N-methyl-N-(4-m...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

methyl iodide Structure

74-88-4

methyl iodide

~%

N-methyl-N-(4-methylsulfanylbuta-1,3-diynyl)aniline Structure

90235-61-3

N-methyl-N-(4-m...

Learn More
1-(3,4,4-trichlorobut-3-en-1-ynyl)pyrrolidine Structure

60014-62-2

1-(3,4,4-trichl...

~%

triphenyl(4-pyrrolidin-1-ylbuta-1,3-diynyl)silane Structure

90235-47-5

triphenyl(4-pyr...

Learn More
Chlorotriphenylsilane Structure

76-86-8

Chlorotriphenyl...

((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

~72%

N-methyl-N-(4-triphenylsilylbuta-1,3-diynyl)aniline Structure

90235-48-6

N-methyl-N-(4-t...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-methyl-N-(4-triphenylsilylbuta-1,3-diynyl)aniline Structure

90235-48-6

N-methyl-N-(4-t...

Learn More
4-(3,4,4-trichlorobut-3-en-1-ynyl)morpholine Structure

60014-60-0

4-(3,4,4-trichl...

~%

4-morpholin-4-ylbuta-1,3-diynyl(triphenyl)stannane Structure

90235-49-7

4-morpholin-4-y...

Learn More
lithium,4-buta-1,3-diynylmorpholine Structure

80487-51-0

lithium,4-buta-...

Fentin chloride Structure

639-58-7

Fentin chloride

~40%

4-morpholin-4-ylbuta-1,3-diynyl(triphenyl)stannane Structure

90235-49-7

4-morpholin-4-y...

Learn More
N-methyl-N-(3,4,4-trichlorobut-3-en-1-ynyl)aniline Structure

82505-76-8

N-methyl-N-(3,4...

~%

N-methyl-N-(4-triphenylstannylbuta-1,3-diynyl)aniline Structure

90235-50-0

N-methyl-N-(4-t...

Learn More
((methyl(phenyl)amino)buta-1,3-diyn-1-yl)lithium Structure

350244-59-6

((methyl(phenyl...

Fentin chloride Structure

639-58-7

Fentin chloride

~21%

N-methyl-N-(4-triphenylstannylbuta-1,3-diynyl)aniline Structure

90235-50-0

N-methyl-N-(4-t...

Learn More

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