Organic preparations and procedures international

An Improved Preparation of S, S'-Dimethyl N-Cyanodithioiminocarbonate

LK Marble

Index: Organic Preparations and Procedures International, , vol. 30, # 4 p. 473 - 476

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Abstract

... The new procedure for the preparation of 3 employs aqueous methanol rather than aqueous ethanol ... which use acetone as a solvent," and the problems associated with preparations in water ... The organic layers were dried (N%SO,), filtered and concentrated in vucuo at 50" to ...