Decarbonylative Radical Cyclization of α-Amino Selenoesters upon Electrophilic Alkenes. A General Method for the 6-Azabicyclo [3.2. 1] octane Synthesis

J Quirante, X Vila, C Escolano…

Index: Journal of Organic Chemistry, , vol. 67, # 7 p. 2323 - 2328

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Citation Number: 44

Abstract

... The Journal of Organic ... The concentrated dried organic extracts were purified by chromatography (CH 2 Cl 2 ) to give 3b (754 mg, 70%) as a yellow solid: IR (KBr) 2200 ... 12, 1H), 2.15−2.53 (m, 4H), 2.96 (m, 1H), 3.38 and 3.42 (2 d, J = 17, 1H each), 3.80 and 3.88 (2 d, J = 13.5, 1H ...