Crystal and molecular structure of 1, 3-dichloro-1, 1, 3, 3-tetraphenyldisilazane

SN Gurkova, AI Gusev, NV Alekseev…

Index: Gurkova, S.N.; Gusev, A. I.; Alekseev, N. V.; Varezhkin, Yu. M. Journal of Structural Chemistry, 1984 , vol. 25, p. 655 - 658 Zhurnal Strukturnoi Khimii, 1984 , vol. 25, # 4 p. 153 - 155

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Citation Number: 2

Abstract

This reaction is not terminated by the stage of formation of compound I: With rising temperature the reaction mixture can yield 1, 3-bis (diphenylchlorosilyl)-2, 2, 4, 4- tetraphenylcyclodisilazane (IV), the crystal structure of which has been studied elsewhere [4]. Fractional recrystallization of the reaction products of 2, 2, 4, 4, 6, 6- hexaphenylcyclotrisilazane and diphenyldichlorosilane from benzene yielded colorless ...