The Journal of Organic Chemistry

Preparation of small-ring carbocycles via intramolecular oxidative coupling of bisenolates derived from. alpha.,. omega.-diesters

JH Babler, SJ Sarussi

Index: Babler, James H.; Sarussi, Steven J. Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3462 - 3464

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Citation Number: 37

Abstract

cessation of Hz evolution). The dichloroacetylene-containing supernatant is virtually free of potassium chloride and residual potassium hydride, which are insoluble in tetrahydrofuran, and hence no distillation is required. The dichloroacetylene so formed has been unambiguously identified by IR (strong absorption at 983 cm-l)* and through known2 chemical transformations: on reaction with imidazole, it produces N-(1, 2-dichlorovinyl) ...

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