Microwave-promoted, one-pot conversion of alkoxymethylated protected alcohols into their corresponding nitriles, bromides, and iodides using [bmim][InCl 4] as a …

A Mirjafari, I Mohammadpoor-Baltork, M Moghadam…

Index: Tetrahedron Letters, , vol. 51, # 25 p. 3274 - 3276

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Citation Number: 18

Abstract

... Please enable JavaScript to use all the features on this page. Tetrahedron Letters. Volume 51, Issue 25, 23 June 2010, Pages 3274–3276. Cover image Cover image. ... Synthesis of Nitriles with Retention of the Cyano Group. Science of Synthesis, Vol. 19, Georg Thieme (2004). ...

 Related Synthetic Route
1-(methoxymethoxymethyl)-4-nitrobenzene Structure

139884-17-6

1-(methoxymetho...

~83%

4-nitrobenzylbromide Structure

100-11-8

4-nitrobenzylbromide

(Methoxymethoxymethyl)benzene Structure

31600-55-2

(Methoxymethoxy...

1-METHOXYMETHYL-1-PHENYLETHANE Structure

94073-86-6

1-METHOXYMETHYL...

~12%

Benzyl bromide Structure

100-39-0

Benzyl bromide

α-Methylbenzyl bromide Structure

585-71-7

α-Methylbenzyl ...

N/A Structure

1058649-04-9

N/A

Tetrabutylammonium cyanide Structure

10442-39-4

Tetrabutylammon...

~79%

(4-Methoxyphenyl)acetonitrile Structure

104-47-2

(4-Methoxypheny...

(Methoxymethoxymethyl)benzene Structure

31600-55-2

(Methoxymethoxy...

1-METHOXYMETHYL-1-PHENYLETHANE Structure

94073-86-6

1-METHOXYMETHYL...

~85%

1-iodoethylbenzene Structure

10604-60-1

1-iodoethylbenzene

(Iodomethyl)benzene Structure

620-05-3

(Iodomethyl)benzene

(Methoxymethoxymethyl)benzene Structure

31600-55-2

(Methoxymethoxy...

1-METHOXYMETHYL-1-PHENYLETHANE Structure

94073-86-6

1-METHOXYMETHYL...

Tetrabutylammonium cyanide Structure

10442-39-4

Tetrabutylammon...

~19%

Benzyl cyanide Structure

140-29-4

Benzyl cyanide

Detail
(Methoxymethoxymethyl)benzene Structure

31600-55-2

(Methoxymethoxy...

~80%

Benzyl bromide Structure

100-39-0

Benzyl bromide

Benzyl(ethoxymethyl) ether Structure

54673-14-2

Benzyl(ethoxyme...

~80%

Benzyl bromide Structure

100-39-0

Benzyl bromide

(Methoxymethoxymethyl)benzene Structure

31600-55-2

(Methoxymethoxy...

1-METHOXYMETHYL-1-PHENYLETHANE Structure

94073-86-6

1-METHOXYMETHYL...

~84%

Benzyl bromide Structure

100-39-0

Benzyl bromide

α-Methylbenzyl bromide Structure

585-71-7

α-Methylbenzyl ...

2,4-dichloro-1-(methoxymethoxy)methyl benzene Structure

877468-98-9

2,4-dichloro-1-...

~77%

1-(Bromomethyl)-2,4-dichlorobenzene Structure

20443-99-6

1-(Bromomethyl)...

2,4-dichloro-1-[(ethoxymethoxy)methyl]benzene Structure

1058649-24-3

2,4-dichloro-1-...

Tetrabutylammonium cyanide Structure

10442-39-4

Tetrabutylammon...

~81%

2,4-Dichlorobenzyl cyanide Structure

6306-60-1

2,4-Dichloroben...

2-methoxy-4-((methoxymethoxy)methyl) phenol Structure

1058649-06-1

2-methoxy-4-((m...

Tetrabutylammonium cyanide Structure

10442-39-4

Tetrabutylammon...

~86%

4-Hydroxy-3-methoxyphenylacetonitrile Structure

4468-59-1

4-Hydroxy-3-met...

4-((ethoxymethoxy)methyl)-2-methoxy phenol Structure

1058649-10-7

4-((ethoxymetho...

Tetrabutylammonium cyanide Structure

10442-39-4

Tetrabutylammon...

~85%

4-Hydroxy-3-methoxyphenylacetonitrile Structure

4468-59-1

4-Hydroxy-3-met...


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