Organic Process Research & Development

Continuous and Batch Organomagnesium Synthesis of Ethyl-Substituted Silanes from Ethylchloride, Tetraethoxysilane, and Organotrichlorosilane for Production of …

BA Klokov

Index: Klokov, Boris A. Organic Process Research and Development, 2001 , vol. 5, # 3 p. 234 - 240

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Citation Number: 6

Abstract

Development of a continuous one-step manufacturing process for ethylethoxy-and ethylchlorosilanes is described. The methodology of synthesis of ethyl-substituted silanes has been improved. The important factors for the successful synthesis have been determined. Among them are (1) the replacement of some tetraethoxysilane 3 by ethyltrichlorosilane 10,(2) the optimum concentration of 3 and 10,(3) the excess of the ...