A convenient one-pot method of converting alcohols into oximes

AR Kiasat, F Kazemi, K Nourbakhsh

Index: Kiasat, Ali Reza; Kazemi, Foad; Nourbakhsh, Kazem Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 9 p. 1809 - 1812

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Citation Number: 2

Abstract

The one-pot conversion of [3pc] primary and secondary alcohols into oximes is reported using chromium trioxide supported on alumina and hydroxylamine hydrochloride under solvent free condition. This oxidation-oxime formation reaction has been applied to a range of aliphatic and benzylic alcohols.

 Related Synthetic Route
(±)-2-Butanol Structure

78-92-2

(±)-2-Butanol

~77%

2-BUTANONE OXIME Structure

96-29-7

2-BUTANONE OXIME

(1r,4r)-4-Phenylcyclohexanol Structure

5769-13-1

(1r,4r)-4-Pheny...

~81%

4-Phenylcyclohexanone oxime Structure

4500-20-3

4-Phenylcyclohe...

Cycloheptanol Structure

502-41-0

Cycloheptanol

~90%

CYCLOHEPTANONE OXIME Structure

2158-31-8

CYCLOHEPTANONE OXIME

4-phenyl-3-buten-2-ol Structure

17488-65-2

4-phenyl-3-bute...

~91%

3-Buten-2-one,4-phenyl-, oxime Structure

2887-98-1

3-Buten-2-one,4...

2-Octanol Structure

4128-31-8

2-Octanol

~79%

2-Octanone, oxime Structure

7207-49-0

2-Octanone, oxime

salicyl alcohol Structure

90-01-7

salicyl alcohol

~69%

salicylaldehyde, oxime Structure

94-67-7

salicylaldehyde...

Cyclohexanol Structure

108-93-0

Cyclohexanol

~70%

Cyclohexanone oxime Structure

100-64-1

Cyclohexanone oxime


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