Photochemistry of the Phthalimide System, 37. Thiazacycloalkanols by Photocyclization of S??Substituted N??(Thioalkyl) phthalimides

Y Sato, H Nakai, M Wada, T Mizoguchi…

Index: Sato, Yasuhiko; Nakai, Hideo; Wada, Masao; Mizoguchi, Tomishige; Hatanaka, Yasumaru; et al. Liebigs Annalen der Chemie, 1985 , # 6 p. 1099 - 1118

Full Text: HTML

Citation Number: 5

Abstract

Abstract N-Substituted phthalimides (1, 2) possessing a terminal thioether function in their side chain were irradiated with a high-pressure mercury lamp to give a variety of thiazacycloalkanol derivatives (3, 7, 9–13, 16, 17) with favored γ-, δ-, ϵ-, and ζ-hydrogen abstractions (Table 1), in moderate to fairly good yields.

~8%

Detail

~77%

~84%

~56%

~17%

~10%

~6%

~6%

~6%

~5%

Thalidomide Analogs from Diamines: Synthesis and Evaluation ...

[De Almeida, Mauro Vieira; Teixeira, Francisco Martins; De Souza, Marcus Vinicius Nora; Amarante, Giovanni Wilson; Alves, Caio Cesar De Souza; Cardoso, Silvia Helena; Mattos, Ana Marcia; Ferreira, Ana Paula; Teixeira, Henrique Couto Chemical and Pharmaceutical Bulletin, 2007 , vol. 55, # 2 p. 223 - 226]

SYNTHÈSE DE NOUVEAUX INITIATEURS. GÉNÉRATION IN SITU DE COMP...

[Lion, Claude; Da Conceicao, Louis; Hedayatullah, Mir Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 161, p. 97 - 113]

SIMPLE AND RAPID SYNTHESIS OF BIOLOGICALLY ACTIVE PHTHALEMID...

[Dalal; Pawar; Mahulikar Organic Preparations and Procedures International, 2007 , vol. 39, # 1 p. 81 - 85]

The reaction of phthalidylidene dichloride with primary amin...

[Guirado, Antonio; Zapata, Andres; Ramirez De Arellano, M. Carmen Tetrahedron, 1997 , vol. 53, # 14 p. 5305 - 5324]

Photolysis experiments on phosmet, an organophosphorus insec...

[Kadam, A. N.; Ghatge, B. B. Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 460 - 461]