Journal of Fluorine Chemistry

Efficient synthesis of p-bis-(chlorodifluoromethyl) benzene

WR Dolbier, JX Duan, XX Rong

Index: Dolbier Jr., William R.; Duan, Jian-Xin; Rong, Xiao X. Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1091 - 1093

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Citation Number: 11

Abstract

Selective, high yield partial fluorination of p-bis-(trichloromethyl) benzene to p-bis- (chlorodifluoromethyl) benzene has been accomplished by warming a slurry of the p-bis- (trichloromethyl) benzene in anhydrous HF which also contains a small quantity of inert solvent, such as 1, 2-dichloroethane.

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