An Efficient Method for Preparation of Chiral Arylmenthol Glyoxylates

…, X García-Mera, C López, JE Rodríguez-Borges…

Index: Blanco, Jose M.; Caamano, Olga; Fernandez, Franco; Garcia-Mera, Xerardo; Lopez, Carmen; Rodriguez-Borges, Jose E.; Hergueta, Antonio R. Synthesis, 1998 , # 11 p. 1590 - 1592

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Citation Number: 8

Abstract

Abstract Glyoxylates of three chiral alcohols were conveniently prepared by reaction of the alcohol with oxalyl chloride followed by reduction of the resulting alkoxy oxalyl chloride with tributyltin hydride. The products were isolated in 75–80% yield by straightforward flash chromatography.

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