Tetrahedron: Asymmetry

Isopropylidene glycerol hydrogen phthalate: a new resolving agent. Application to the resolution of 1-arylethylamines

M Pallavicini, E Valoti, L Villa, O Piccolo

Index: Pallavicini, Marco; Valoti, Ermanno; Villa, Luigi; Piccolo, Oreste Tetrahedron Asymmetry, 1996 , vol. 7, # 4 p. 1117 - 1122

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Citation Number: 21

Abstract

Hydrogen phthalates of (R)-and (S)-isopropylidene glycerol, obtainable from racemic isopropylidene glycerol by reaction with phthalic anhydride and successive resolution with (S)-and (R)-1-phenylethylamine or, alternatively, from (R)-and (S)-isopropylidene glycerol, were regarded as potential new resolving agents. A range of important 1-arylethylamines was selected to test their resolving capability. In particular, trial resolutions were carried ...

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