Tetrachlorophthalic anhydride

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Names

[ CAS No. ]:
117-08-8

[ Name ]:
Tetrachlorophthalic anhydride

[Synonym ]:
4,5,6,7-Tetrachloro-1,3-isobenzofurandione
1,3-Isobenzofurandione, 4,5,6,7-tetrachloro-
Tetrachlorophthalic anhydride
4,5,6,7-Tetrachloro-2-benzofuran-1,3-dione
MFCD00005920
EINECS 204-171-4

Chemical & Physical Properties

[ Density]:
1.9±0.1 g/cm3

[ Boiling Point ]:
371.0±0.0 °C at 760 mmHg

[ Melting Point ]:
253-257 °C(lit.)

[ Molecular Formula ]:
C8Cl4O3

[ Molecular Weight ]:
285.896

[ Flash Point ]:
161.6±25.5 °C

[ Exact Mass ]:
283.860168

[ PSA ]:
43.37000

[ LogP ]:
3.56

[ Vapour Pressure ]:
0.0±0.8 mmHg at 25°C

[ Index of Refraction ]:
1.656

[ Stability ]:
Stable. Reacts with water. Combustible. Incompatible with strong oxidizing agents. Air and moisture sensitive.

[ Water Solubility ]:
0.8 mg/L (21 ºC)

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
TI3450000
CHEMICAL NAME :
Phthalic anhydride, tetrachloro-
CAS REGISTRY NUMBER :
117-08-8
BEILSTEIN REFERENCE NO. :
0211560
LAST UPDATED :
199712
DATA ITEMS CITED :
12
MOLECULAR FORMULA :
C8-Cl4-O3
MOLECULAR WEIGHT :
285.88

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
Standard Draize test
ROUTE OF EXPOSURE :
Administration into the eye
SPECIES OBSERVED :
Rodent - rabbit
REFERENCE :
NTPTR* National Toxicology Program Technical Report Series. (Research Triangle Park, NC 27709) No.206- Volume(issue)/page/year: NIH-93-3351 ** ACUTE TOXICITY DATA **
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
>15800 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
NTPTR* National Toxicology Program Technical Report Series. (Research Triangle Park, NC 27709) No.206- Volume(issue)/page/year: NIH-93-3351
TYPE OF TEST :
LC - Lethal concentration
ROUTE OF EXPOSURE :
Inhalation
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
>3600 mg/m3/4H
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
NTPTR* National Toxicology Program Technical Report Series. (Research Triangle Park, NC 27709) No.206- Volume(issue)/page/year: NIH-93-3351
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rabbit
DOSE/DURATION :
>5 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
NTPTR* National Toxicology Program Technical Report Series. (Research Triangle Park, NC 27709) No.206- Volume(issue)/page/year: NIH-93-3351 ** OTHER MULTIPLE DOSE TOXICITY DATA **
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
68250 mg/kg/13W-I
TOXIC EFFECTS :
Liver - changes in liver weight Kidney, Ureter, Bladder - changes in tubules (including acute renal failure, acute tubular necrosis) Related to Chronic Data - death
REFERENCE :
NTPTR* National Toxicology Program Technical Report Series. (Research Triangle Park, NC 27709) No.206- Volume(issue)/page/year: NIH-93-3351
TYPE OF TEST :
TCLo - Lowest published toxic concentration
ROUTE OF EXPOSURE :
Inhalation
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
5 mg/m3/6H/13W-I
TOXIC EFFECTS :
Lungs, Thorax, or Respiration - changes in lung weight Endocrine - hyperglycemia Blood - changes in leukocyte (WBC) count
REFERENCE :
NTIS** National Technical Information Service. (Springfield, VA 22161) Formerly U.S. Clearinghouse for Scientific & Technical Information. Volume(issue)/page/year: OTS0538630 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOHS - National Occupational Hazard Survey (1974) NOHS Hazard Code - M3316 No. of Facilities: 55 (estimated) No. of Industries: 2 No. of Occupations: 3 No. of Employees: 142 (estimated) NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - M3316 No. of Facilities: 43 (estimated) No. of Industries: 4 No. of Occupations: 6 No. of Employees: 2067 (estimated) No. of Female Employees: 786 (estimated)

Safety Information

[ Symbol ]:

GHS05, GHS08, GHS09

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H317-H318-H334-H350-H373-H410

[ Precautionary Statements ]:
P201-P261-P273-P280-P305 + P351 + P338-P308 + P313

[ Hazard Codes ]:
T:Toxic

[ Risk Phrases ]:
R41;R42/43;R45;R50/53

[ Safety Phrases ]:
S53-S22-S24-S26-S37/39-S45-S60-S61

[ RIDADR ]:
UN 3077 9/PG 3

[ WGK Germany ]:
2

[ RTECS ]:
TI3450000

[ Packaging Group ]:
III

[ Hazard Class ]:
9

[ HS Code ]:
2917399090

Synthetic Route

Precursor & DownStream

Precursor

  • Phthalic anhydride
  • Tetrachlorophthalic acid
  • 3,4,5,6-Tetrachlorphthalsaeure-bis(4-chlorphenyl)ester
  • Naphthalene
  • Perchlor-bicyclo[4.2.0]octatrien-(1.5.7)
  • 2,3,4,5,7,8-Hexachlorbicyclo[4.2.0]octa-1,3,5-trien-7,8-diylsulfat
  • Sulfuric acid
  • Benzoic acid,2,3,4,5-tetrachloro-6-[(diethylamino)carbonyl]-

DownStream

  • N-Phenyltetrachlorophthalimide
  • N-Methyltetrafluorophthalimide
  • TCID
  • 2,3,4,5-Tetrachlorobenzoic acid
  • methyl 2,3,4,5-tetrachlorobenzoate
  • N,N-dimethyl-2,3,4,5-tetrachlorobenzamide
  • 2,3,4,5-Tetrachlorobenzoyl chloride
  • 3,6-Dichlorophthalic anhydride
  • 2,4,5-Trifluorobenzoic acid
  • 2',4',5',7'-Tetrabromo-4,5,6,7-tetrachloro-3',6'-dihydroxy-3H-spi ro[2-benzofuran-1,9'-xanthen]-3-one

Customs

[ HS Code ]: 2932999099

[ Summary ]:
2932999099. other heterocyclic compounds with oxygen hetero-atom(s) only. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%

Articles

Allergic reactions to industrial chemicals.

Clin. Immunol. Rev. 2(1) , 1-58, (1983)

Acid anhydrides.

Clin. Exp. Allergy 21 Suppl 1 , 234-40, (1991)

Immunologic specificity of IgG against trimellityl-human serum albumin in serum samples of workers exposed to trimellitic anhydride.

J. Lab. Clin. Med. 121(6) , 792-6, (1993)

The specificity of immunoglobulin G (IgG) against trimellityl-human serum albumin (TM-HSA) in serum samples from 11 workers exposed to trimellitic anhydride (TMA) was characterized in this study. Leve...


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Related Compounds

  • naphthalene-tetrachlorophthalic anhydride
  • Tetrachlorophthalic anhydride,glycerin,ethylene glycol polymer
  • Ethylene glycol,maleic anhydride,tetrachlorophthalic anhydride
  • Methyloxirane,phosphoric acid,tetrachlorophthalic anhydride polymer
  • Tetrachlorophthalic anhydride,phthalic anhydride,adipic acid,ethylene glycol polymer
  • Tetrachlorophthalic acid hydrogen 1-(1-phenylpentyl) ester
  • 4-((Cyclohexylamino)methyl)benzoic acid hydrochloride
  • 1-[(2,4-Dichlorophenyl)methyl]-N-(1,1-dimethylethyl)-2-methyl-1H-indole-3-methanamine
  • 2-Methoxy-6-(pyrazol-1-yl)-benzonitrile
  • 4-(Tert-butoxy)-3-methylbutan-1-amine
  • 1H-3-Benzazepin-7-ol, 8-chloro-2,3,4,5-tetrahydro-5-(3-iodophenyl)-3-methyl-, (S)-
  • (4-Methyl-tetrahydro-furan-2-yl)-methanol
  • N-(1-cyanocyclopentyl)-2-[4-(4-fluorobenzenesulfonyl)-1,4-diazepan-1-yl]acetamide
  • 4,5,6,7-Tetrahydrobenzo[d]isoxazole-3-carbaldehyde
  • 2-{1-[2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-1,3-thiazol-4-yl]-N-(2-methylpropyl)formamido}acetic acid
  • tert-Butyl-DL-alanine