Trimethyl phosphite

Suppliers

Names

[ CAS No. ]:
121-45-9

[ Name ]:
Trimethyl phosphite

[Synonym ]:
Methyl phosphite (P(OMe)3
dimethyl methylphosphonate
Trimethylfosfit
Trimethylphosphite
Methyl phosphite
Trimethyl phosphite
Fosforyn trojmetylowy
MFCD00008350
EINECS 204-471-5
Trimethoxyphosphine
Phosphorous acid, trimethyl ester
phosphorous acid trimethyl ester

Chemical & Physical Properties

[ Density]:
1.052 g/mL at 25 °C(lit.)

[ Boiling Point ]:
110.2±8.0 °C at 760 mmHg

[ Melting Point ]:
−78 °C(lit.)

[ Molecular Formula ]:
C3H9O3P

[ Molecular Weight ]:
124.076

[ Flash Point ]:
27.8±0.0 °C

[ Exact Mass ]:
124.028931

[ PSA ]:
41.28000

[ LogP ]:
-0.93

[ Vapour density ]:
4.3 (vs air)

[ Vapour Pressure ]:
28.1±0.2 mmHg at 25°C

[ Index of Refraction ]:
n20/D 1.408(lit.)

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
TH1400000
CHEMICAL NAME :
Phosphorous acid, trimethyl ester
CAS REGISTRY NUMBER :
121-45-9
LAST UPDATED :
199712
DATA ITEMS CITED :
29
MOLECULAR FORMULA :
C3-H9-O3-P
MOLECULAR WEIGHT :
124.09
WISWESSER LINE NOTATION :
1OPO1&O1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
Standard Draize test
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rabbit
REFERENCE :
34ZIAG "Toxicology of Drugs and Chemicals," Deichmann, W.B., New York, Academic Press, Inc., 1969 Volume(issue)/page/year: -,609,1969
TYPE OF TEST :
Standard Draize test
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Mammal - species unspecified
REFERENCE :
MEPAAX Medycyna Pracy. Industrial Medicine. (Ars-Polona, POB 1001, 00-068 Warsaw 1, Poland) V.1- 1950- Volume(issue)/page/year: 29,393,1978
TYPE OF TEST :
Standard Draize test
ROUTE OF EXPOSURE :
Administration into the eye
SPECIES OBSERVED :
Mammal - species unspecified
REFERENCE :
MEPAAX Medycyna Pracy. Industrial Medicine. (Ars-Polona, POB 1001, 00-068 Warsaw 1, Poland) V.1- 1950- Volume(issue)/page/year: 29,393,1978 ** ACUTE TOXICITY DATA **
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
1600 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
ALBRW* Albright & Wilson Inc. (P.O. Box 26229, Richmond, VA 23260-6229) Volume(issue)/page/year: #OPB-3,1984
TYPE OF TEST :
LC50 - Lethal concentration, 50 percent kill
ROUTE OF EXPOSURE :
Inhalation
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
>10000 ppm/4H
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
AIHAAP American Industrial Hygiene Association Journal. (AIHA, 475 Wolf Ledges Pkwy., Akron, OH 44311) V.19- 1958- Volume(issue)/page/year: 34,286,1973
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
4180 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
ENVRAL Environmental Research. (Academic Press, Inc., 1 E. First St., Duluth, MN 55802) V.1- 1967- Volume(issue)/page/year: 9,1,1975
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rabbit
DOSE/DURATION :
2600 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
AIHAAP American Industrial Hygiene Association Journal. (AIHA, 475 Wolf Ledges Pkwy., Akron, OH 44311) V.19- 1958- Volume(issue)/page/year: 34,286,1973 ** OTHER MULTIPLE DOSE TOXICITY DATA **
TYPE OF TEST :
TCLo - Lowest published toxic concentration
ROUTE OF EXPOSURE :
Inhalation
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
500 ppm/7.5H/8W-I
TOXIC EFFECTS :
Lungs, Thorax, or Respiration - emphysema Lungs, Thorax, or Respiration - fibrosis, focal (pneumoconiosis) Skin and Appendages - hair
REFERENCE :
AIHAAP American Industrial Hygiene Association Journal. (AIHA, 475 Wolf Ledges Pkwy., Akron, OH 44311) V.19- 1958- Volume(issue)/page/year: 34,286,1973 ** REPRODUCTIVE DATA **
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
1640 mg/kg
SEX/DURATION :
female 6-15 day(s) after conception
TOXIC EFFECTS :
Reproductive - Specific Developmental Abnormalities - Central Nervous System Reproductive - Specific Developmental Abnormalities - craniofacial (including nose and tongue) Reproductive - Specific Developmental Abnormalities - musculoskeletal system
REFERENCE :
TXAPA9 Toxicology and Applied Pharmacology. (Academic Press, Inc., 1 E. First St., Duluth, MN 55802) V.1- 1959- Volume(issue)/page/year: 72,119,1984
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
1640 mg/kg
SEX/DURATION :
female 6-15 day(s) after conception
REFERENCE :
TXAPA9 Toxicology and Applied Pharmacology. (Academic Press, Inc., 1 E. First St., Duluth, MN 55802) V.1- 1959- Volume(issue)/page/year: 72,119,1984 *** REVIEWS *** ACGIH TLV-TWA 10 mg/m3 (2 ppm) DTLVS* The Threshold Limit Values (TLVs) and Biological Exposure Indices (BEIs) booklet issues by American Conference of Governmental Industrial Hygienists (ACGIH), Cincinnati, OH, 1996 Volume(issue)/page/year: TLV/BEI,1997 *** OCCUPATIONAL EXPOSURE LIMITS *** OEL-AUSTRALIA:TWA 2 ppm (10 mg/m3) JAN 1993 OEL-BELGIUM:TWA 2 ppm (10 mg/m3) JAN 1993 OEL-DENMARK:TWA 0.5 ppm (2.6 mg/m3) JAN 1993 OEL-FINLAND:TWA 0.5 ppm (2.6 mg/m3);STEL 10 ppm (52 mg/m3);Skin JAN 1993 OEL-FRANCE:TWA 2 ppm (10 mg/m3) JAN 1993 OEL-THE NETHERLANDS:TWA 2 ppm (10 mg/m3) JAN 1993 OEL-SWITZERLAND:TWA 2 ppm (10 mg/m3) JAN 1993 OEL-UNITED KINGDOM:TWA 2 ppm (10 mg/m3) JAN 1993 OEL IN BULGARIA, COLOMBIA, JORDAN, KOREA check ACGIH TLV OEL IN NEW ZEALAND, SINGAPORE, VIETNAM check ACGIH TLV *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH RECOMMENDED EXPOSURE LEVEL (REL) : NIOSH REL TO TRIMETHYL PHOSPHITE-air:10H TWA 2 ppm REFERENCE : NIOSH* National Institute for Occupational Safety and Health, U.S. Dept. of Health, Education, and Welfare, Reports and Memoranda. Volume(issue)/page/year: DHHS #92-100,1992 NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOHS - National Occupational Hazard Survey (1974) NOHS Hazard Code - 84215 No. of Facilities: 260 (estimated) No. of Industries: 5 No. of Occupations: 7 No. of Employees: 1891 (estimated) NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - 84215 No. of Facilities: 55 (estimated) No. of Industries: 2 No. of Occupations: 18 No. of Employees: 14190 (estimated) No. of Female Employees: 6312 (estimated)

Safety Information

[ Symbol ]:

GHS02, GHS05, GHS07

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H226-H302-H315-H318-H335

[ Supplemental HS ]:
Reacts violently with water.

[ Precautionary Statements ]:
P261-P280-P305 + P351 + P338

[ Personal Protective Equipment ]:
Eyeshields;Faceshields;full-face respirator (US);Gloves;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ Hazard Codes ]:
Xn:Harmful;

[ Risk Phrases ]:
R10;R22;R36/37/38

[ Safety Phrases ]:
S26

[ RIDADR ]:
UN 2329 3/PG 3

[ WGK Germany ]:
1

[ RTECS ]:
TH1400000

[ Packaging Group ]:
III

[ Hazard Class ]:
3

[ HS Code ]:
2920901100

Synthetic Route

Precursor & DownStream

Precursor

  • Methanol
  • pentacarbonyl(trimethylphosphite)chromium(0)
  • Tetraphosphorus nonoxide
  • tetraphosphorus octaoxide
  • tris(4-dimethylaminopyridine)phosphorus(3+) bromide
  • lithium,methoxyethyne
  • DIMETHYLCHLOROPHOSPHITE
  • Sodium Methylate
  • Dimethyl phosphonate
  • 4',4'-dimethyl-2λ5-spiro[benzo[1,3,2]dioxaphosphole-2,2'-[1,3,2]oxazaphospholidin]-5'-one

DownStream

  • (1-chloropropylideneamino) dimethyl phosphate
  • Phosphonic acid,P-(4-methoxybenzoyl)-, dimethyl ester
  • 2-chloro-4-dimethoxyphosphoryl-6-methoxy-1,3,5-triazine
  • 11-(2,5-dimethyl-11-bicyclo[4.4.1]undeca-3,7,9-trienyl)-2,5-dimethylbicyclo[4.4.1]undeca-3,7,9-triene
  • Dichlorvos
  • Metrifonate
  • 2,2-dichloroethenyl methyl hydrogen phosphate
  • Methanol
  • 4-methoxyphenylphosphonic acid diethyl ester

Customs

[ HS Code ]: 2920901100

[ Summary ]:
2920901100 trimethyl phosphite。supervision conditions:23(import license for dual-use item and technologies,export license for dual-use item and technologies)。VAT:17.0%。tax rebate rate:9.0%。MFN tarrif:6.5%。general tariff:30.0%

Articles

Interactions of multitargeted kinase inhibitors and nucleoside drugs: Achilles heel of combination therapy?

J. Chromatogr. A. 1421 , 154-61, (2015)

Multitargeted tyrosine kinase inhibitors (TKI) axitinib, pazopanib, and sunitinib are used to treat many solid tumors. Combination trials of TKIs with gemcitabine, a nucleoside anticancer drug, in pan...

Rapid modification of the insect elicitor N-linolenoyl-glutamate via a lipoxygenase-mediated mechanism on Nicotiana attenuata leaves.

BMC Plant Biol. 10 , 164, (2010)

Some plants distinguish mechanical wounding from herbivore attack by recognizing specific constituents of larval oral secretions (OS) which are introduced into plant wounds during feeding. Fatty acid-...

The functionalisation of saturated hydrocarbons--XXX. Model studies on the mechanism of some oxygenases.

Bioorg. Med. Chem. 2(4) , 259-66, (1994)

In harmony with our studies on the activation of hydrocarbons by Gif chemistry, we have, in the first part of this paper, studied the mechanism of the lipoxygenase enzymes using soybean lipoxygenase a...


More Articles


Related Compounds

  • trimethyl phosphite-d9
  • Pt(trimethyl phosphite)4
  • trimethyl phosphite ozonide
  • [W(CO)5(trimethyl phosphite)]
  • iodo(trimethyl phosphite-P)copper
  • Iron,tetracarbonyl(trimethyl phosphite-P)-
  • 4-((Cyclohexylamino)methyl)benzoic acid hydrochloride
  • 2-Ethyl-4,5-dimethylthieno[2,3-d]pyrimidine-6-carboxylic acid
  • 1-[(2,4-Dichlorophenyl)methyl]-N-(1,1-dimethylethyl)-2-methyl-1H-indole-3-methanamine
  • 4-(Benzyloxycarbonyl)-1-isopropylpiperazine-2-carboxylic acid
  • 2-Methoxy-6-(pyrazol-1-yl)-benzonitrile
  • 1H-3-Benzazepin-7-ol, 8-chloro-2,3,4,5-tetrahydro-5-(3-iodophenyl)-3-methyl-, (S)-
  • (4-Methyl-tetrahydro-furan-2-yl)-methanol
  • N-(1-cyanocyclopentyl)-2-[4-(4-fluorobenzenesulfonyl)-1,4-diazepan-1-yl]acetamide
  • 4,5,6,7-Tetrahydrobenzo[d]isoxazole-3-carbaldehyde
  • tert-Butyl-DL-alanine