2'-Iodoacetophenone

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Names

[ CAS No. ]:
2142-70-3

[ Name ]:
2'-Iodoacetophenone

[Synonym ]:
1-(2-iodophenyl)ethan-1-one
2-IC6H4COMe
2′-Iodoacetophenone
MFCD00094998
2-Ac-C6H4-I
2‘-Iodoacetophenone
o-Iodoacetophenone
ortho-iodoacetophenone
2'-Iodoacetophenone
2-Iodoacetophenone
2'-IODO-1,1':3',1''-TERPHENYL
o-acetyl-iodobenzene
1-acetyl-2-iodobenzene
Acetophenone,o-iodo
1-(2-Iodophenyl)ethanone

Chemical & Physical Properties

[ Density]:
1.72 g/mL at 25 °C(lit.)

[ Boiling Point ]:
139-140°C 12mm

[ Molecular Formula ]:
C8H7IO

[ Molecular Weight ]:
246.04500

[ Flash Point ]:
218 °F

[ Exact Mass ]:
245.95400

[ PSA ]:
17.07000

[ LogP ]:
2.49380

[ Vapour Pressure ]:
0.00779mmHg at 25°C

[ Index of Refraction ]:
n20/D 1.618(lit.)

MSDS

Click to get detail MSDS

Safety Information

[ Personal Protective Equipment ]:
Eyeshields;Gloves;half-mask respirator (US);multi-purpose combination respirator cartridge (US)

[ Hazard Codes ]:
C: Corrosive;

[ Risk Phrases ]:
R36/38

[ Safety Phrases ]:
S26-S36

[ RIDADR ]:
NONH for all modes of transport

[ WGK Germany ]:
3

[ HS Code ]:
2914700090

Synthetic Route

Click to get detail synthetic route

Precursor & DownStream

Precursor

  • 2'-Aminoacetophenone
  • diiodobenzene
  • Ethanoic anhydride
  • Acetophenone
  • (+/-)-1-(2-iodophenyl)-ethanol
  • 1-Chloro-1,3-dihydro-3,3-dimethyl-1,2-benziodoxole
  • 2-Iodobenzaldehyde
  • METHYLMAGNESIUM IODIDE
  • 2-Iodobenzoyl chloride

DownStream

  • Benzoic acid,2-acetyl-, methyl ester
  • 2'-Aminoacetophenone
  • Methyl 4-acetylbenzoate
  • (R)-α-(Hydroxymethyl)benzeneacetic acid methyl ester
  • Acetophenone
  • [N-(trifluoromethanesulfonyl)imino][2-(acetyl)phenyl]-λ3-iodane
  • 4-Bromobenzotrifluoride
  • 3-Methyl-1H-indazole
  • 9-Methylacridine
  • Ortho-Hydroxyacetophenone

Customs

[ HS Code ]: 2914700090

[ Summary ]:
HS: 2914700090 halogenated, sulphonated, nitrated or nitrosated derivatives of ketones and quinones, whether or not with other oxygen function Tax rebate rate:9.0% Supervision conditions:none VAT:17.0% MFN tariff:5.5% General tariff:30.0%

Articles

Trapping evidence for the thermal cyclization of di-(o-acetylphenyl)acetylene to 3,3'-dimethyl-1,1'-biisobenzofuran.

Beilstein J. Org. Chem. 1(1) , 18, (2005)

The reaction of di-(o-acetylphenyl)acetylene (1) with excess dimethyl acetylenedicarboxylate (DMAD) produced bis-DMAD adducts meso-3 and rac-3. This transformation is suggested to involve thermal rear...

Cobalt-catalyzed regioselective carbocyclization reaction of o-iodophenyl ketones and aldehydes with alkynes, acrylates, and acrylonitrile: a facile route to indenols and indenes.

J. Org. Chem. 69(14) , 4781-7, (2004)

An efficient cobalt-catalyzed carbocylization for the synthesis of indenols and indenes and a new method for reductive decyanation are described. 2-Iodophenyl ketones and aldehydes 1a-g undergo carboc...

Cobalt-Catalyzed Carbocyclization of o-Iodobenzaldehydes and o-Iodophenylketones with Alkynes. Chang KJ, et al.

Org. Lett. 5(21) , 3963-3966, (2003)


More Articles

Related Compounds

  • 2'-IODOACETOPHENONE
  • 5'-Fluoro-2'-iodoacetophenone
  • 2-(3-BROMOPHENYL)-2'-IODOACETOPHENONE
  • 2-(4-BROMOPHENYL)-2'-IODOACETOPHENONE
  • 2-(4-CYANOPHENYL)-2'-IODOACETOPHENONE
  • 2-(3-BROMOPHENYL)-2'-IODOACETOPHENONE
  • 4-Fluorophenyl 3-phenyl-5,6-dihydro-1,4-oxathiine-2-carboxylate 4,4-dioxide
  • 1,5-dioxo-N-[(2Z)-5-(propan-2-yl)-1,3,4-thiadiazol-2(3H)-ylidene]-4-propyl-2,3,4,5-tetrahydropyrrolo[1,2-a]quinazoline-3a(1H)-carboxamide
  • N1-(4-methylpiperazin-1-yl)-N2-(4-(trifluoromethyl)phenyl)oxalamide
  • 4-(4-oxoquinazolin-3(4H)-yl)-N-[(2Z)-5-(2-phenylethyl)-1,3,4-thiadiazol-2(3H)-ylidene]butanamide
  • 6-Chloro-n4-methyl-n4-((1-methyl-1h-pyrazol-4-yl)methyl)pyrimidine-2,4-diamine
  • 2-[2-(2,3-dihydro-1,4-benzodioxin-6-yl)-2-oxoethyl]-6-(4-fluorophenyl)pyridazin-3(2H)-one
  • 2-(3,4-dimethoxyphenyl)-4-methyl-N-[(2E)-5-methyl-1,3,4-thiadiazol-2(3H)-ylidene]-1,3-thiazole-5-carboxamide
  • 1-methyl-N-(2-phenylethyl)-1H-indole-5-carboxamide
  • [5-(2-Chlorophenyl)thiophen-2-yl](thiomorpholin-4-yl)methanone
  • 6-(furan-2-yl)-2-[2-oxo-2-(1,2,6-trimethyl-1H-indol-3-yl)ethyl]pyridazin-3(2H)-one
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