((R)-2,2-Dimethyl-1,3-dioxolan-4-yl)methyl p-toluenesulfonate

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Names

[ Name ]:
((R)-2,2-Dimethyl-1,3-dioxolan-4-yl)methyl p-toluenesulfonate

[Synonym ]:
(R)-(-)-2,2-dimethyl-4-tosyloxymethyl-1,3-dioxolane
(R)-(-)-2,2-dimethyl-4-(hydroxymethyl)-1,3-dioxolane-p-toluenesulfonate
(R)-2,2-dimethyl-1,3-dioxolan-4-methanol toluene-4-sulfonate
MFCD00063233
(R)-2,2-Dimethyl-1,3-dioxolane-4-methanol p-toluenesulfonate
[(4R)-2,2-Dimethyl-1,3-dioxolan-4-yl]methyl 4-methylbenzenesulfonate
1,3-Dioxolane-4-methanol, 2,2-dimethyl-, 4-methylbenzenesulfonate, (4R)-
(R)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl toluene-4-sulfonate
(R)-1-(2,2-dimethyl-1,3-dioxolan-4-yl)methyl 4-methyl-benzenesulfonate
(4R)-2,2-dimethyl-4-(4-toluenesulphonyloxymethyl)-1,3-dioxolane
(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)methyl 4-methylbenzenesulfonate
(R)-(-)-2,2-DIMETHYL-1,3-DIOXOLAN-4-YLMETHYL P-TOLUENESULFONATE
(R)-(-)-2,2-Dimethyl-1,3-dioxolan-4-ylmethylp-Toluenesulfonate
(R)-(-)-2,2-Dimethyl-1,3-dioxolane-4-ylmethyl-p-toluenesulfonate
(R)-2,2-dimethyl-1,3-dioxolan-4-ylmethyl p-tosylate
1,2-Isopropylidene-sn-glycerol 3-tosylate
(R)-(2,2-DIMETHYL-1,3-DIOXOLAN-4-YL)METHYL-4-METHYLBENZENESULFONATE
((R)-2,2-Dimethyl-1,3-dioxolan-4-yl)methyl p-toluenesulfonate
p-Toluenesulfonic acid [(R)-2,2-dimethyl-1,3-dioxolane-4β-yl]methyl ester

Chemical & Physical Properties

[ Density]:
1.2±0.1 g/cm3

[ Boiling Point ]:
400.1±25.0 °C at 760 mmHg

[ Melting Point ]:
41-43 °C(lit.)

[ Molecular Formula ]:
C₁₃H₁₈O₅S

[ Molecular Weight ]:
286.344

[ Flash Point ]:
195.8±23.2 °C

[ Exact Mass ]:
286.087494

[ PSA ]:
70.21000

[ LogP ]:
1.58

[ Vapour Pressure ]:
0.0±0.9 mmHg at 25°C

[ Index of Refraction ]:
1.507

[ Storage condition ]:
−20°C

MSDS

Click to get detail MSDS

Safety Information

[ Personal Protective Equipment ]:
dust mask type N95 (US);Eyeshields;Gloves

[ Hazard Codes ]:
Xn: Harmful;Xi: Irritant;

[ Risk Phrases ]:
R36/37/38

[ Safety Phrases ]:
S26-S36-S37/39

[ RIDADR ]:
NONH for all modes of transport

[ WGK Germany ]:
3

[ HS Code ]:
2932999099

Synthetic Route

Click to get detail synthetic route

Precursor & DownStream

Precursor

(S)-(+)-Solketal
Tosyl chloride
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol
(R)-(-)-Solketal
(R)-(+)-2,2-Dimethyl-1,3-dioxolane-4-carboxaldehyde

DownStream

(R)-Glycerol 1-(p-toluenesulfonate)
4-[[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl]morpholine
(S)-N-(2,2-DIMETHYL-1[1,3]DIOXOLAN-4-YLMETHYL)-ACETAMIDE
(S)-(-)-PROPYLENEOXIDE
2,2-dimethyl-4(s)-4-azidomethyl-1,3-dioxalane
sodium,2-methylphenolate
1-O-Hexadecyl-sn-glycerol

Customs

[ HS Code ]: 2932999099

[ Summary ]:
2932999099. other heterocyclic compounds with oxygen hetero-atom(s) only. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%

Articles

C. André et al.

Tetrahedron Asymmetry 9 , 1359, (1998)

K.C. Nicolaou et al.

J. Chem. Soc. Chem. Commun. , 349, (1984)

S.K. Bhatia, J. Hajdu

Tetrahedron Lett. 28 , 1729, (1987)

4-(1-Hydroxy-3-methoxy-2-methylpropan-2-yl)-1-methylpiperidin-4-ol
(2R)-2-[(2R)-2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-3-methylbutanamido]-4-methoxy-4-oxobutanoic acid
rac-(1R,3S)-3-{2-[({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)methyl]pentanamido}cyclopentane-1-carboxylic acid
4-[2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-(methoxymethyl)propanamido]oxolane-3-carboxylic acid
1-[3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)pentanoyl]-2-methylpiperidine-4-carboxylic acid
5-({1-[({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)methyl]cyclobutyl}formamido)-2-methylpentanoic acid
2-[4-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-3-methoxy-N-(2-methoxyethyl)butanamido]acetic acid
4-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-5-[4-(methylsulfanyl)piperidin-1-yl]-5-oxopentanoic acid
4-[5-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-4-methylpentanamido]-3-methoxybutanoic acid
2-{1-[2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)hex-4-ynoyl]piperidin-3-yl}acetic acid

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