Aminopicoline

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Names

[ CAS No. ]:
695-34-1

[ Name ]:
Aminopicoline

[Synonym ]:
2-amino-4-Me-pyridine
2-Amino-4-meyhylpyrimidine
MFCD00149166
2-Pyridinamine,4-methyl
4-methyl-pyridin-2-ylamine
4-Methyl-2-aminopyridine
2-Amino-4-methylpyridine
2-Amino-4-picoline
2-amino-4-methyl-pyridine
4-Methylpyridin-2-amin
EINECS 234-190-3
Ascensil
4-Methyl-2-pyridylamine
2-Pyridinamine, 4-methyl-
4-PICOLINAMINE
4-PICOLINE,2-AMINO
4-Methyl-2-pyridinamine
4-Methylpyridin-2-amine

Chemical & Physical Properties

[ Density]:
1.1±0.1 g/cm3

[ Boiling Point ]:
227.4±20.0 °C at 760 mmHg

[ Melting Point ]:
96-99 °C(lit.)

[ Molecular Formula ]:
C6H8N2

[ Molecular Weight ]:
108.141

[ Flash Point ]:
114.0±9.0 °C

[ Exact Mass ]:
108.068748

[ PSA ]:
38.91000

[ LogP ]:
1.08

[ Vapour Pressure ]:
0.1±0.4 mmHg at 25°C

[ Index of Refraction ]:
1.574

[ Water Solubility ]:
SOLUBLE

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
TJ5150000
CHEMICAL NAME :
4-Picoline, 2-amino-
CAS REGISTRY NUMBER :
695-34-1
BEILSTEIN REFERENCE NO. :
0107066
LAST UPDATED :
199701
DATA ITEMS CITED :
6
MOLECULAR FORMULA :
C6-H8-N2
MOLECULAR WEIGHT :
108.16
WISWESSER LINE NOTATION :
T6NJ BZ D1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
200 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
85JCAE "Prehled Prumyslove Toxikologie; Organicke Latky," Marhold, J., Prague, Czechoslovakia, Avicenum, 1986 Volume(issue)/page/year: -,841,1986
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Subcutaneous
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
160 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
AEPPAE Naunyn-Schmiedeberg's Archiv fuer Experimentelle Pathologie und Pharmakologie. (Berlin, Ger.) V.110-253, 1925-66. For publisher information, see NSAPCC. Volume(issue)/page/year: 227,234,1955
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Subcutaneous
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
64 mg/kg
TOXIC EFFECTS :
Behavioral - convulsions or effect on seizure threshold Behavioral - excitement
REFERENCE :
NYKZAU Nippon Yakurigaku Zasshi. Japanese Journal of Pharmacology. (Nippon Yakuri Gakkai, c/o Kyoto Daigaku Igakubu Yakurigaku Kyoshitsu, Konoe-cho, Yoshida, Sakyo-ku, Kyoto 606, Japan) V.40- 1944- Volume(issue)/page/year: 53,227S,1957
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intravenous
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
39 mg/kg
TOXIC EFFECTS :
Behavioral - convulsions or effect on seizure threshold
REFERENCE :
APFRAD Annales Pharmaceutiques Francaises. (SPPIF, B.P.22, F-41353 Vineuil, France) V.1- 1943- Volume(issue)/page/year: 26,345,1968
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - guinea pig
DOSE/DURATION :
500 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
85JCAE "Prehled Prumyslove Toxikologie; Organicke Latky," Marhold, J., Prague, Czechoslovakia, Avicenum, 1986 Volume(issue)/page/year: -,841,1986

Safety Information

[ Symbol ]:

GHS06, GHS08

[ Signal Word ]:
Danger

[ Hazard Statements ]:
H301 + H311 + H331-H373

[ Precautionary Statements ]:
P261-P280-P301 + P310-P311

[ Personal Protective Equipment ]:
Eyeshields;Faceshields;Gloves;type P2 (EN 143) respirator cartridges

[ Hazard Codes ]:
T:Toxic

[ Risk Phrases ]:
R25;R36/37/38

[ Safety Phrases ]:
S53-S45-S60-S61-S37/39-S28A-S26-S36/37/39

[ RIDADR ]:
UN 3086 6.1/PG 1

[ WGK Germany ]:
3

[ RTECS ]:
TJ5150000

[ Packaging Group ]:
II

[ Hazard Class ]:
6.1

[ HS Code ]:
2932999099

Synthetic Route

Precursor & DownStream

Precursor

  • 2-(2,5-dimethylpyrrol-1-yl)-4-methylpyridine
  • 4-picoline n-oxide
  • 2,2-dimethyl-3-(4-methylpyrid-2-yl)-4-oxo-4H-1,3-benzoxazine
  • 4-Picoline
  • 4-methyl(2-nitroso)pyridine

DownStream

  • 2-methoxy-6-[[(4-methylpyridin-2-yl)amino]methylidene]cyclohexa-2,4-dien-1-one
  • 2-[4-(trichloromethyl)pyridin-2-yl]isoindole-1,3-dione
  • 4-Methyl-2-phenylpyridine
  • 2-Chloro-4-picoline
  • 2-Methoxy-4-methylpyridine
  • 2-Acetylaminoisonicotinic acid
  • 2-Bromo-4-methylpyridine
  • 2-Bromo-4-(bromomethyl)pyridine
  • 2-Fluor-3-iod-6-methylpyridin
  • Methyl 2-fluoroisonicotinate

Customs

[ HS Code ]: 2933399090

[ Summary ]:
2933399090. other compounds containing an unfused pyridine ring (whether or not hydrogenated) in the structure. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%

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Related Compounds

  • 5-aminopicoline
  • 3-aminopicoline
  • Aminopicoline-d6
  • 4-((Cyclohexylamino)methyl)benzoic acid hydrochloride
  • 1-[(2,4-Dichlorophenyl)methyl]-N-(1,1-dimethylethyl)-2-methyl-1H-indole-3-methanamine
  • 2-Methoxy-6-(pyrazol-1-yl)-benzonitrile
  • 1,1-Difluoro-2-methyl-3-(4-methylpyridin-3-yl)propan-2-amine
  • 3-(1-ethyl-1H-pyrazol-3-yl)-5-methoxy-5-oxopentanoic acid
  • 1H-3-Benzazepin-7-ol, 8-chloro-2,3,4,5-tetrahydro-5-(3-iodophenyl)-3-methyl-, (S)-
  • (4-Methyl-tetrahydro-furan-2-yl)-methanol
  • N-(1-cyanocyclopentyl)-2-[4-(4-fluorobenzenesulfonyl)-1,4-diazepan-1-yl]acetamide
  • 4,5,6,7-Tetrahydrobenzo[d]isoxazole-3-carbaldehyde
  • tert-Butyl-DL-alanine