L-Histidine

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Names

[ CAS No. ]:
71-00-1

[ Name ]:
L-Histidine

[Synonym ]:
(S)-a-Amino-1H-imidazole-4-propanoic Acid
(S)-1H-Imidazole-4-alanine
a-Amino-4(or 5)-Imidazolepropionic Acid
d,l-histidine
1H-Imidazole-4-propanoic acid, α-amino-, (S)-
FEMA 3694
(S)-histidine
EINECS 200-745-3
HISTIDINE, L-
His
Histidine
H-L-HIS-OH
3-(1H-imidazol-4-yl)-L-Alanine
hydrogen L-histidinate
L-His
Histidin
L-Histdine
L-Hisidine
MFCD00064315
L-Histidine
H-His-OH

Chemical & Physical Properties

[ Density]:
1.4±0.1 g/cm3

[ Boiling Point ]:
458.9±35.0 °C at 760 mmHg

[ Melting Point ]:
282 °C (dec.)(lit.)

[ Molecular Formula ]:
C6H9N3O2

[ Molecular Weight ]:
155.155

[ Flash Point ]:
231.3±25.9 °C

[ Exact Mass ]:
155.069473

[ PSA ]:
92.00000

[ LogP ]:
-1.26

[ Vapour Pressure ]:
0.0±1.2 mmHg at 25°C

[ Index of Refraction ]:
1.615

[ Water Solubility ]:
41.6 g/L (25 ºC)

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
MS3070000
CHEMICAL NAME :
Histidine, L-
CAS REGISTRY NUMBER :
71-00-1
LAST UPDATED :
199709
DATA ITEMS CITED :
18
MOLECULAR FORMULA :
C6-H9-N3-O2
MOLECULAR WEIGHT :
155.18
WISWESSER LINE NOTATION :
T5M CNJ E1YZVQ

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
>15 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
>8 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Subcutaneous
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
>10 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intravenous
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
>2 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
>15 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
>10 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Subcutaneous
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
>10 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intravenous
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
>2 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
221 gm/kg/46D-C
TOXIC EFFECTS :
Liver - changes in liver weight Blood - other changes Nutritional and Gross Metabolic - changes in metals, not otherwise specified
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
12 gm/kg/5W-I
TOXIC EFFECTS :
Kidney, Ureter, Bladder - other changes Endocrine - changes in adrenal weight Blood - changes in serum composition (e.g. TP, bilirubin, cholesterol)
TYPE OF TEST :
Cytogenetic analysis

MUTATION DATA

TYPE OF TEST :
Cytogenetic analysis
TEST SYSTEM :
Rodent - hamster Lung
DOSE/DURATION :
2500 ppm
REFERENCE :
TOLED5 Toxicology Letters. (Elsevier Science Pub. B.V., POB 211, 1000 AE Amsterdam, Netherlands) V.1- 1977- Volume(issue)/page/year: 28,117,1985 *** OCCUPATIONAL EXPOSURE LIMITS *** OEL-RUSSIA:STEL 2 mg/m3 JAN 1993 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - X4775 No. of Facilities: 233 (estimated) No. of Industries: 2 No. of Occupations: 8 No. of Employees: 13683 (estimated) No. of Female Employees: 11508 (estimated)

Safety Information

[ Personal Protective Equipment ]:
Eyeshields;Gloves;type N95 (US);type P1 (EN143) respirator filter

[ Hazard Codes ]:
Xn: Harmful;

[ Risk Phrases ]:
22-36/37/38

[ Safety Phrases ]:
S24/25

[ RIDADR ]:
NONH for all modes of transport

[ WGK Germany ]:
2

[ RTECS ]:
MS3070000

[ HS Code ]:
2933290090

Synthetic Route

Precursor & DownStream

Precursor

  • L-carnosine
  • L-2-Thiolhistidine
  • L-Histidine
  • H-His(Trt)-OH
  • methyl (2S)-2-amino-3-(1H-imidazol-5-yl)propanoate
  • BOC-HIS(BOM)-OH
  • Boc-His(Tos)-OH
  • Gly-His
  • N-Acetyl-DL-histidine hydrate
  • H-His(MBS)-OH

DownStream

  • L-Histidine,N-(2,4-dinitrophenyl)-
  • cucumopine
  • Mikimopine
  • Boc-His(Trt)-OH
  • 3-Methyl-L-histidine
  • 1-Methyl-L-histidine
  • Boc-His(Boc)-OH DCHA
  • H-His(Trt)-OH
  • L-Histidine,N,1-bis(2,4-dinitrophenyl)-

Customs

[ HS Code ]: 2933290090

[ Summary ]:
2933290090. other compounds containing an unfused imidazole ring (whether or not hydrogenated) in the structure. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%

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Related Compounds

  • L-Histidine
  • bzl-histidine
  • L-Histidine Base
  • L-Histidine-15N3
  • poly-l-histidine
  • arginyl-histidine
  • (4-isopropyl-1H-imidazol-5-yl)methanol
  • 3-(4-Bromophenyl)-4-methyl-1H-pyrazole
  • [2-Chloro-5-(trifluoromethyl)phenyl]cyanamide
  • 4-(trifluoromethyl)pyrimidine-2-sulfonyl Chloride
  • 1-(1,2-Dimethyl-1H-indol-3-yl)-1-butanone
  • N-Methyl-N2-[[(4-nitrophenyl)methoxy]carbonyl]-D-asparagine
  • 1,2-Bis((4-fluorophenyl)thio)ethane
  • 5-(3-Chloro-4-fluorophenyl)-1,3,4-thiadiazol-2-amine
  • 2-(Dicarbethoxymethyl)-quinoxaline
  • (2R,4R)-N,2-Diphenyl-3,4-dihydro-2H-1-benzopyran-4-amine
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